Analytical techniques for high-mass materials: Method development
作者： Rafael Kandiyoti , Alan Herod , Keith Bartle , Trevor Morgan
DOI: 10.1016/B978-0-08-100784-6.00007-2
关键词: Mass spectrometry 、 Column chromatography 、 Gas chromatography 、 Analytical chemistry 、 Desorption 、 Size-exclusion chromatography 、 Fourier transform ion cyclotron resonance 、 Chemistry 、 Asphaltene 、 Fourier transform infrared spectroscopy
摘要: This chapter describes analytical chemical methods used to characterize high-mass materials found in liquids and tars from coal processing crude petroleum fractions such as asphaltenes the conversion of biomass into liquid fuels. Methods described include size exclusion chromatography with different solvents, mass spectrometric method including laser desorption, nuclear magnetic resonance, fractionation techniques, vapour pressure osmometry, UV-fluorescence Fourier Transform infrared spectroscopy. Significant developments these fields are described. Comparison ion cyclotron resonance spectrometry (FT-ICR-MS) reveals significant shortcomings that application residues. The components have previously been ignored.
sci-hub.se 参考文章(496)
Magnetic resonance of carbonaceous solids American Chemical Society. ,(1992) , 10.1021/BA-1993-0229
P. Torregrosa-Rodrı́guez, M. Martı́nez-Escandell, F. Rodrı́guez-Reinoso, H. Marsh, C.Gómez de Salazar, E.Romero Palazón, Pyrolysis of petroleum residues: II. Chemistry of pyrolysis Carbon. ,vol. 38, pp. 535- 546 ,(2000) , 10.1016/S0008-6223(99)00133-5
Eric Y. Sheu, M. M. De Tar, D. A. Storm, Surface Activity And Dynamics Of Asphaltenes Springer, Boston, MA. pp. 115- 122 ,(1994) , 10.1007/978-1-4615-2456-4_9
G. Haberhauer, W. Bednar, M.H. Gerzabek, E. Rosenberg, MALDI-TOF-MS analysis of humic substances - a new approach to obtain additional structural information? Understanding Humic Substances#R##N#Advanced Methods, Properties and Applications. pp. 121- 128 ,(1999) , 10.1016/B978-1-85573-815-7.50017-9
Sheng-Fu Zhang, Bin Xu, Alan A. Herod, Geoff M. Kimber, Denis R. Dugwell, Rafael Kandiyoti, Effect of coal rank on hydrocracking reactivities of primary coal extracts prepared in a flowing-solvent reactor: The Argonne premium coal sample set Fuel. ,vol. 75, pp. 1557- 1567 ,(1996) , 10.1016/0016-2361(96)00119-6
W. Li, T.J. Morgan, A.A. Herod, R. Kandiyoti, Thin-layer chromatography of pitch and a petroleum vacuum residue: Relation between mobility and molecular size shown by size-exclusion chromatography Journal of Chromatography A. ,vol. 1024, pp. 227- 243 ,(2004) , 10.1016/J.CHROMA.2003.10.020
Robert J. Evans, Thomas A. Milne, Molecular characterization of the pyrolysis of biomass Energy & Fuels. ,vol. 1, pp. 123- 137 ,(1987) , 10.1021/EF00002A001
Yuqun Zhuo, Alan A. Herod, Rafael Kandiyoti, Thermochemical Reactions of Middle Rank Coals Springer, Dordrecht. pp. 53- 151 ,(2003) , 10.1007/978-94-017-0111-2_3
AR Lea-Langton, GE Andrews, KD Bartle, JM Jones, A Williams, None, Combustion and pyrolysis reactions of alkylated polycyclic aromatic compounds: The decomposition of 13C methylarenes in relation to diesel engine emissions Fuel. ,vol. 158, pp. 719- 724 ,(2015) , 10.1016/J.FUEL.2015.05.043
Norman G. Foster, Mynard C. Hamming, Interpretation of mass spectra of organic compounds ,(1972)