Rapid method for esterification of trace levels of carboxylic acids for analysis by gas chromatography--electron-capture detection.
作者： R.D. Mortimer
DOI: 10.1016/S0021-9673(01)89283-9
关键词: Electron capture 、 Derivatization 、 Carboxylic acid 、 Trace analysis 、 Electron capture detector 、 Gas chromatography 、 Chromatography 、 Chemistry
摘要: On a utilise l'esterification des acides carboxyliques avec l'hexafluoroisopropanol comme moyen simple et rapide pour prepare derives volatils de ces en vue leur analyse par GC-ECD
elsevier.com
sci-hub.se 参考文章(10)
Bruce J. Balcom, Nils O. Petersen, Solvent dependence of carboxylic acid condensations with dicyclohexylcarbodiimide Journal of Organic Chemistry. ,vol. 54, pp. 1922- 1927 ,(1989) , 10.1021/JO00269A032
Larry S. Trzupek, Anita Go, Kenneth D. Kopple, Hexafluoro-2-propyl esters in peptide synthesis Journal of Organic Chemistry. ,vol. 44, pp. 4577- 4581 ,(1979) , 10.1021/JO00393A025
Bernard Carre, Jacques Devynck, None, The acidity functions of trifluoroethanol and hexafluoroisopropanol, and their mixtures with water Analytica Chimica Acta. ,vol. 131, pp. 141- 147 ,(1981) , 10.1016/S0003-2670(01)93544-5
Tadashi Tsukioka, Tetsuro Murakami, Capillary gas chromatographic-mass spectrometric determination of acid herbicides in soils and sediments. Journal of Chromatography A. ,vol. 469, pp. 351- 359 ,(1989) , 10.1016/S0021-9673(01)96469-6
Richard F. Arrendale, James T. Stewart, Randall Manning, Banjong Vitayavirasuk, Determination of GX-071 and its major metabolite in rat blood by cold on-column injection capillary GC/ECD Journal of Agricultural and Food Chemistry. ,vol. 37, pp. 1130- 1135 ,(1989) , 10.1021/JF00088A069
B.A. Davis, D.A. Durden, P. Pun-Li, A.A. Boulton, Gas chromatographic procedure for the determination of meta- and para-hydroxyphenylacetic acids Journal of Chromatography A. ,vol. 142, pp. 517- 522 ,(1977) , 10.1016/S0021-9673(01)92064-3
Marian Mikoz.xl;lajczyk, Piotr Kiez.xl;lbasiński, Recent developments in the carbodiimide chemistry Tetrahedron. ,vol. 37, pp. 233- 284 ,(1981) , 10.1016/S0040-4020(01)92010-1
Elisabet Fogelqvist, Bjørn Josefsson, Claes Roos, Determination of carboxylic acids and phenols in water by extractive alkylation using pentafluorobenzylation, glass capillary GC and electron capture detection Hrc-journal of High Resolution Chromatography. ,vol. 3, pp. 568- 574 ,(1980) , 10.1002/JHRC.1240031105
Robert J. Strife, Robert C. Murphy, Preparation of pentafluorobenzyl esters of arachidonic acid lipoxygenase metabolites Journal of Chromatography B: Biomedical Sciences and Applications. ,vol. 305, pp. 3- 12 ,(1984) , 10.1016/S0378-4347(00)83309-5
Michael A. Brook, T. H. Chan, A Simple Procedure for the Esterification of Carboxylic Acids Synthesis. ,vol. 1983, pp. 201- 203 ,(1983) , 10.1055/S-1983-30279