Application of two-phase hollow fiber liquid phase microextraction coupled with high-performance liquid chromatography for the study of the echinacoside pharmacokinetics in Parkinson's disease rat plasma
作者： Jun Zhou , Ping Zeng , Jiang Bing Sun , Feng Qiao Wang , Qiong Zhang
DOI: 10.1016/J.JPBA.2013.03.020
关键词: Chemistry 、 Echinacoside 、 Calibration curve 、 High-performance liquid chromatography 、 Fiber 、 Detection limit 、 Analyte 、 Chromatography 、 Sample preparation 、 Analytical chemistry 、 Pharmacokinetics 、 Spectroscopy 、 Clinical biochemistry 、 Drug discovery 、 Pharmaceutical Science
摘要: Abstract A simple and solvent-minimized sample preparation technique based on two-phase hollow fiber liquid phase microextraction (HF-LPME) was developed used to quantify the echinacoside in Parkinson's disease rat plasma following oral administration. Analysis accomplished by reversed-phase high performance chromatography (HPLC) with ultraviolet detection. The influence factors relevant HF-LPME processes were optimized. Under optimized conditions, preconcentration factor for 337. Calibration curves reasonable linearity ( r 2 ≥ 0.9998) obtained range of 5–750 ng mL −1 . Intra-day inter-day precision (RSD) ≤5.43% limit detection (LOD) analyte 2.0 ng mL (S/N = 3). validated method has been successfully applied pharmacokinetic studies (PD) after
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sci-hub.se 参考文章(26)
VA Kurkin, None, Phenylpropanoids from Medicinal Plants: Distribution, Classification, Structural Analysis, and Biological Activity Chemistry of Natural Compounds. ,vol. 39, pp. 123- 153 ,(2003) , 10.1023/A:1024876810579
Peng Fei Tu, Yong Jiang, Ming Zhong, Juan Du, Liu Fei, Chun Yang Liu, Hong Chen, Lei Wang, Li Li Wei, Effects of echinacoside on histio-central levels of active mass in middle cerebral artery occlusion rats. Biomedical and Environmental Sciences. ,vol. 25, pp. 238- 244 ,(2012) , 10.3967/0895-3988.2012.02.017
Abolfazl Saleh, Estelle Larsson, Yadollah Yamini, Jan Åke Jönsson, None, Hollow fiber liquid phase microextraction as a preconcentration and clean-up step after pressurized hot water extraction for the determination of non-steroidal anti-inflammatory drugs in sewage sludge Journal of Chromatography A. ,vol. 1218, pp. 1331- 1339 ,(2011) , 10.1016/J.CHROMA.2011.01.011
Miguel Ángel Bello-López, María Ramos-Payán, Juan Antonio Ocaña-González, Rut Fernández-Torres, Manuel Callejón-Mochón, Analytical Applications of Hollow Fiber Liquid Phase Microextraction (HF-LPME): A Review Analytical Letters. ,vol. 45, pp. 804- 830 ,(2012) , 10.1080/00032719.2012.655676
Min Zhu, Chuanzhen Lu, Wenwei Li, Transient exposure to echinacoside is sufficient to activate Trk signaling and protect neuronal cells from rotenone Journal of Neurochemistry. ,vol. 124, pp. 571- 580 ,(2013) , 10.1111/JNC.12103
Hong Chen, Fu Chun Jing, Chang Ling Li, Peng Fei Tu, Qiu Sheng Zheng, Zheng Hua Wang, Echinacoside prevents the striatal extracellular levels of monoamine neurotransmitters from diminution in 6-hydroxydopamine lesion rats. Journal of Ethnopharmacology. ,vol. 114, pp. 285- 289 ,(2007) , 10.1016/J.JEP.2007.07.035
Cunqin Jia, Haiming Shi, Xiangmei Wu, Yinzeng Li, Jingjing Chen, Pengfei Tu, Determination of echinacoside in rat serum by reversed-phase high-performance liquid chromatography with ultraviolet detection and its application to pharmacokinetics and bioavailability. Journal of Chromatography B. ,vol. 844, pp. 308- 313 ,(2006) , 10.1016/J.JCHROMB.2006.07.040
Dimitra A. Lambropoulou, Triantafyllos A. Albanis, Liquid-phase micro-extraction techniques in pesticide residue analysis. Journal of Biochemical and Biophysical Methods. ,vol. 70, pp. 195- 228 ,(2007) , 10.1016/J.JBBM.2006.10.004
Rong Kuang, Yiguo Sun, Wei Yuan, Li Lei, Xiaoxiang Zheng, Protective Effects of Echinacoside, One of the Phenylethanoid Glycosides, on H2O2-Induced Cytotoxicity in PC12 Cells Planta Medica. ,vol. 75, pp. 1499- 1504 ,(2009) , 10.1055/S-0029-1185806
Jun Zhou, Ping Zeng, Zhao Hui Cheng, Jing Liu, Feng Qiao Wang, Ruo Jun Qian, Application of hollow fiber liquid phase microextraction coupled with high-performance liquid chromatography for the study of the osthole pharmacokinetics in cerebral ischemia hypoperfusion rat plasma Journal of Chromatography B. ,vol. 879, pp. 2304- 2310 ,(2011) , 10.1016/J.JCHROMB.2011.06.022