作者: Darwish Amin , Sadallah T. Sulaiman
DOI: 10.1039/AN9840900739
关键词: Iodate 、 Phenols 、 Polarography 、 Resorcinol 、 Iodide 、 Halogenation 、 Catechol 、 Phloroglucinol 、 Chromatography 、 Chemistry
摘要: Simple titrimetric, spectrophotometric and polarographic methods are described for the determination of micro-amounts resorcinol, catechol phloroglucinol. These based on iodination above compounds in a buffered solution which resulting iodide, after removal excess iodine, is oxidised with bromine to give iodate, determined titrimetrically, spectrophotometrically or polarographically. An time 1 min at pH 5.7 used resorcinol 4 The ranges 10–1 000 µg 20–1 phloroglucinol by titrimetric method, 5–30 method 1–1 method.