Gas-chromatographic determination of methylester end groups in polyethylene terephthalate (PET) and ester-interchange products

作者: D. Vink , R. Wijk

DOI: 10.1007/BF00426418

关键词: HydratePolyethylene terephthalateBackflush accountingMethanolPolyesterTenaxHydrazineChemistryChromatographyGas chromatography

摘要: A method for the determination of methylester end groups in polyester and ester-interchange product is described. The sample decomposed by boiling with hydrazine hydrate. methanol liberated determined gas chromatography using Tenax GC as column packing ethanol internal standard. chromatographic has passed through a number development stages, viz. backflush run methods.

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R. van Wijk, The Use of Poly-Para-2, 6-Diphenyl-Phenylene Oxide as a Porous Polymer in Gas Chromatography Journal of Chromatographic Science. ,vol. 8, pp. 418- 420 ,(1970) , 10.1093/CHROMSCI/8.7.418