The gas chromatographic analysis of some polycondensation polymers
作者： O. Mleinek , Ľ. Cvečková
DOI: 10.1016/S0021-9673(01)92362-3
关键词:
摘要: Abstract A method for the identification of basic constituents polyesters, polyimides and polymides, alond in combination with each other, is proposed. It consists splitting polymers into parent monomers followed by their gas chromatographic analysis. For amines polyalcohols, analysis acids, hydrazinolysis mainolysis tetramethylammonium hydroxide, respectively, are recommended. The reaction conditions were studied various discussed.
elsevier.com
sci-hub.se 参考文章(13)
D. Vink, R. Wijk, Gas-chromatographic determination of methylester end groups in polyethylene terephthalate (PET) and ester-interchange products Fresenius Journal of Analytical Chemistry. ,vol. 264, pp. 293- 296 ,(1973) , 10.1007/BF00426418
E. W. Robb, J. J. Westbrook, Preparation of Methyl Esters for Gas Liquid Chromatography of Acids by Pyrolysis of Tetramethylammonium salts. Analytical Chemistry. ,vol. 35, pp. 1644- 1647 ,(1963) , 10.1021/AC60204A029
E. D. Bitner, Alan C. Lanser, H. J. Dutton, Alkali isomerization—Gas chromatography with the microreactor apparatus Journal of the American Oil Chemists' Society. ,vol. 48, pp. 633- 635 ,(1971) , 10.1007/BF02544578
Hanns G. Henkel, Phenolätherbildung im Einspritzblock eines Gaschromatographen Journal of Chromatography A. ,vol. 20, pp. 596- 597 ,(1965) , 10.1016/S0021-9673(01)97466-7
Joseph John. Bailey, Determination of aliphatic and aromatic acids by pyrolysis of their tetramethylammonium salts Analytical Chemistry. ,vol. 39, pp. 1485- 1489 ,(1967) , 10.1021/AC60256A044
Donald T. Downing, Analysis of aqueous solutions of organic acids by pyrolysis of their tetramethylammonium salts in the gas chromatograph Analytical Chemistry. ,vol. 39, pp. 218- 221 ,(1967) , 10.1021/AC60246A026
J. W. Schwarze, Marion N. Gilmour, Gas-chromatographic determination of C1 to C7 monocarboxylic acids and lactic acid by pyrolysis of the tetrabutyl ammonium salts Analytical Chemistry. ,vol. 41, pp. 1686- 1687 ,(1969) , 10.1021/AC60281A038
George W. Stevenson, On-column methylation of barbituric acids. Analytical Chemistry. ,vol. 38, pp. 1948- 1949 ,(1966) , 10.1021/AC50155A076
Donald T. Downing, Richard S. Greene, Methylation of fatty acids by pyrolysis of their tetramethylammonium salts in the gas chromatograph. Analytical Chemistry. ,vol. 40, pp. 827- 828 ,(1968) , 10.1021/AC60260A035
N. E. Hetman, H. G. Arlt, R. Paylor, R. Feinland, Gas chromatographic analysis of tall oil rosin acids Journal of the American Oil Chemists' Society. ,vol. 42, pp. 255- 256 ,(1965) , 10.1007/BF02541143