Microstructural Evolution and Mechanical Properties of ZrB2–SiC/Cu/Ti/Ti6Al4V Brazing Joints†

作者: Weiqi Yang , Peng He , Lili Xing , Tiesong Lin

DOI: 10.1002/ADEM.201500281

关键词: BrazingShear strengthIndentation hardnessTitanium alloyWhiskersMetallurgyEnergy-dispersive X-ray spectroscopyMaterials scienceCeramicMicrostructure

摘要: A joint of ZrB2-SiC ceramic to Ti6Al4V alloy was achieved successfully by contact reactive brazing with Ti/Cu lamination. The microstructure and chemical composition joining interfaces were investigated electron backscattered diffraction, energy dispersive spectroscopy X-ray diffraction. results revealed that ZrB2 had much faster decomposing velocity than SiC in Ti–Cu liquid alloy. Two types distribution TiB whiskers produced on surface due different growing conditions. microstructural evolution temperatures analyzed. mechanical properties the joints evaluated microhardness shear tests. maximum strength reached 90.7 MPa temperature at 920 °C for 10 min.

参考文章(19)
Kirsten Bobzin, Mehmet Öte, Stefanie Wiesner, Anke Kaletsch, Christoph Broeckmann, Characterization of Reactive Air Brazed Ceramic/Metal Joints with Unadapted Thermal Expansion Behavior Advanced Engineering Materials. ,vol. 16, pp. 1490- 1497 ,(2014) , 10.1002/ADEM.201400311
W. F. Gale, E. R. Wallach, Microstructural development in transient liquid-phase bonding Metallurgical Transactions A. ,vol. 22, pp. 2451- 2457 ,(1991) , 10.1007/BF02665011
Weiqi Yang, Tiesong Lin, Peng He, Yudong Huang, Jicai Feng, Microstructural investigation of in situ TiB whiskers array reinforced ZrB2–SiC joint Journal of Alloys and Compounds. ,vol. 527, pp. 117- 121 ,(2012) , 10.1016/J.JALLCOM.2012.03.016
M. Singh, R. Asthana, Joining of zirconium diboride-based ultra high-temperature ceramic composites using metallic glass interlayers Materials Science and Engineering A-structural Materials Properties Microstructure and Processing. ,vol. 460, pp. 153- 162 ,(2007) , 10.1016/J.MSEA.2007.01.015
Peng He, Weiqi Yang, Tiesong Lin, Dechang Jia, Jicai Feng, Yu Liu, Diffusion bonding of ZrB2–SiC/Nb with in situ synthesized TiB whiskers array Journal of the European Ceramic Society. ,vol. 32, pp. 4447- 4454 ,(2012) , 10.1016/J.JEURCERAMSOC.2012.07.005
Norihiko L. Okamoto, Misato Kusakari, Katsushi Tanaka, Haruyuki Inui, Masaharu Yamaguchi, Shigeki Otani, Temperature dependence of thermal expansion and elastic constants of single crystals of ZrB2 and the suitability of ZrB2 as a substrate for GaN film Journal of Applied Physics. ,vol. 93, pp. 88- 93 ,(2003) , 10.1063/1.1525404
C. Paturaud, G. Farges, M.C. Sainte Catherine, J. Machet, Influence of sputtering gases on the properties of magnetron sputtered tungsten films Surface and Coatings Technology. ,vol. 86-87, pp. 388- 393 ,(1996) , 10.1016/S0257-8972(96)02954-4
N. H. Salpadoru, H. M. Flower, Phase equilibria and transformations in a Ti-Zr-Si system Metallurgical and Materials Transactions A-physical Metallurgy and Materials Science. ,vol. 26, pp. 243- 257 ,(1995) , 10.1007/BF02664663
Jin Hui Xiong, Ji Hua Huang, Hua Zhang, Xing Ke Zhao, Brazing of carbon fiber reinforced SiC composite and TC4 using Ag–Cu–Ti active brazing alloy Materials Science and Engineering A-structural Materials Properties Microstructure and Processing. ,vol. 527, pp. 1096- 1101 ,(2010) , 10.1016/J.MSEA.2009.09.024
Frederic Monteverde, Stefano Guicciardi, Alida Bellosi, Advances in microstructure and mechanical properties of zirconium diboride based ceramics Materials Science and Engineering A-structural Materials Properties Microstructure and Processing. ,vol. 346, pp. 310- 319 ,(2003) , 10.1016/S0921-5093(02)00520-8