Synthesis of silver nanoparticles by gelcasting using a low toxic monomer and optimization of gelation time using the Taguchi method
作者： Mehrdad Manteghian , Hassan Pahlavanzadeh , Ali Askari Zadeh Mahani
DOI: 10.1080/02726351.2016.1154907
关键词: Chemical engineering 、 Taguchi methods 、 Polymer chemistry 、 Calcination 、 Materials science 、 Monomer 、 Nanoparticle 、 Scanning electron microscope 、 Methacrylamide 、 Silver nanoparticle 、 In situ polymerization
摘要: ABSTRACTSilver nanoparticles were synthesized using a gelcasting process, which includes in situ polymerization for forming the samples followed by calcination. Methacrylamide (MAM) was used as monomer and N,N′-methylene-bis-acrylamide (MBAM) cross-linker to form cross-linked polymer network. The effects of content, ratio, silver salt ratio on gelation time investigated Taguchi experimental design method. A set 16 experiments conducted at constant temperature agitation speed. results from Minitab (DOE) analysis indicate that had greatest effect time. Finally, burning out gel sample furnace. Scanning electron microscopy (SEM) showed average size approximately 42 nm.
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