Synthesis and characterisation of titanosilicate ETS-10 membranes

作者: Zhi Lin , João Rocha , Alberto Navajas , Carlos Téllez , Joaquı́n Coronas

DOI: 10.1016/J.MICROMESO.2003.10.004

关键词: Aluminium oxidesPervaporationMembraneScanning electron microscopeChemical engineeringPorosityMineralogyMolecular sieveZeoliteHydrothermal synthesisMaterials science

摘要: Abstract Titanosilicate ETS-10 membranes have been prepared on porous α-alumina and stainless steel tubular supports by seeded hydrothermal synthesis. The influence of synthesis conditions has studied, pure ≈5 μm thick were synthesised, exhibiting a good intergrowth crystals. characterised X-ray diffraction, scanning electron microscopy, energy dispersive spectrometry mapping. Pervaporation experiments performed, yielding at 150 °C water/ethanol separation factor up to 12 water flux 1.1 kg/(m2 h).

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