Isolation of natural products by low-pressure column chromatography.

作者: Raymond G. Reid , Satyajit D. Sarker

DOI: 10.1007/978-1-61779-624-1_7

关键词: Size-exclusion chromatographyPlant ComponentsAdsorptionChromatographyColumn chromatographyChemistryChromatography column

摘要: This chapter describes the isolation of natural products using low-pressure column chromatography (LPLC) and provides a brief summary adsorption size exclusion processes involved in LPLC. Different types stationary phases used both LPLC are also presented with specific examples. Various operational parameters relation to packing (both wet dry), equilibration, sample application, development, generic procedures for incorporated this chapter. Throughout chapter, several examples application various including alkaloids, coumarins, flavones, saponins from plants given. Many these include combination obtain compounds.

参考文章(114)
Satyajit D. Sarker, James A. Armstrong, Peter G. Waterman, (−)-1,12-oxagual-10(15)-ene: A sesquiterpene from Eriostemon fitzgeraldii Phytochemistry. ,vol. 40, pp. 1159- 1162 ,(1995) , 10.1016/0031-9422(95)00382-H
Mohammad Shoeb, Stephen M. MacManus, Yashodharan Kumarasamy, Marcel Jaspars, Lutfun Nahar, Paul Kong Thoo-Lin, Hossein Nazemiyeh, Satyajit D. Sarker, Americanin, a bioactive dibenzylbutyrolactone lignan, from the seeds of Centaurea americana. Phytochemistry. ,vol. 67, pp. 2370- 2375 ,(2006) , 10.1016/J.PHYTOCHEM.2006.08.012
Kyeong Yeol Oh, Jin Hwan Lee, Marcus J. Curtis-Long, Jung Keun Cho, Jun Young Kim, Woo Song Lee, Ki Hun Park, Glycosidase inhibitory phenolic compounds from the seed of Psoralea corylifolia Food Chemistry. ,vol. 121, pp. 940- 945 ,(2010) , 10.1016/J.FOODCHEM.2010.01.022
Satyajit D Sarker, Pensri Whiting, Laurence Dinan, Vladimir Šik, Huw H Rees, Identification and ecdysteroid antagonist activity of three resveratrol trimers (suffruticosols A, B and C) from Paeonia suffruticosa Tetrahedron. ,vol. 55, pp. 513- 524 ,(1999) , 10.1016/S0040-4020(98)01049-7
Supayang P. Voravuthikunchai, Tripetch Kanchanapoom, Nongyao Sawangjaroen, Nongporn Hutadilok-Towatana, Antioxidant, antibacterial and antigiardial activities of Walsura robusta Roxb. Natural Product Research. ,vol. 24, pp. 813- 824 ,(2010) , 10.1080/14786410902819152
Jesús G Díaz, Juan García Ruiz, Gabriel de la Fuente, None, Alkaloids from Delphinium staphisagria. Journal of Natural Products. ,vol. 63, pp. 1136- 1139 ,(2000) , 10.1021/NP990453L
Satyajit D. Sarker, Tamara Savchenko, Pensri Whiting, Vladimir Šik, Laurence Dinan, Two limonoids from Turraea obtusifolia (Meliaceae), prieurianin and rohitukin, antagonise 20-hydroxyecdysone action in a Drosophila cell line. Archives of Insect Biochemistry and Physiology. ,vol. 35, pp. 211- 217 ,(1997) , 10.1002/(SICI)1520-6327(1997)35:1/2<211::AID-ARCH19>3.0.CO;2-E
Amiram Groweiss, John H. Cardellina, Michael R. Boyd, HIV-inhibitory prenylated xanthones and flavones from Maclura tinctoria. Journal of Natural Products. ,vol. 63, pp. 1537- 1539 ,(2000) , 10.1021/NP000175M
Charles A Ferguson, Lutfun Nahar, Douglas Finnie, Yashodharan Kumarasamy, Raymond Reid, Namik F Mir-Babayev, Satyajit D Sarker, Centaurea scabiosa: a source of dibenzylbutyrolactone lignans Biochemical Systematics and Ecology. ,vol. 31, pp. 303- 305 ,(2003) , 10.1016/S0305-1978(02)00143-6
Masoud Modaressi, Abbas Delazar, Hossein Nazemiyeh, Fatemeh Fathi-Azad, Eileen Smith, M. Mukhlesur Rahman, Simon Gibbons, Lutfun Nahar, Satyajit D. Sarker, Antibacterial iridoid glucosides from Eremostachys laciniata Phytotherapy Research. ,vol. 23, pp. 99- 103 ,(2009) , 10.1002/PTR.2568