Smooth or not: Robust fused silica micro-components by femtosecond-laser-assisted etching

作者: Johann Michler , Jakob Schwiedrzik , David Bischof , Jakub Jurczyk , Jakub Jurczyk

DOI: 10.1016/J.MATDES.2021.109670

关键词: Materials scienceEtching (microfabrication)MicrometreOrders of magnitude (numbers)Annealing (glass)Finite element methodFemtosecondStress concentrationComposite materialFabrication

摘要: Abstract Recent progress in manufacturing now enables the efficient fabrication of complex oxide-glass components at micrometer– to sub-micrometer scale. This benefits both industry and fundamental research as such miniature glass parts have numerous applications. However, these length-scales, mechanical properties glasses can no longer be predicted based on bulk material characteristics. Here it is shown that fused silica micro-pillars fabricated by laser-assisted etching are almost ten times stronger than their bulk-sized counterparts. The relatively rough surface typical for this process does not much impair strength. Additionally, demonstrated annealing as-fabricated structures 1200 °C air results significantly smoother surfaces. accompanying increase strength from approximately 8 GPa 10 due reduction stress concentrations surface, finite element simulations. It also gain resistance downsizing occurs already large 20 µm – orders magnitude above critical size reported other micro-mechanical effects. These selective structured key a reliable use micro-components.

参考文章(59)
Dong Wu, Si‐Zhu Wu, Jian Xu, Li‐Gang Niu, Katsumi Midorikawa, Koji Sugioka, Hybrid femtosecond laser microfabrication to achieve true 3D glass/polymer composite biochips with multiscale features and high performance: the concept of ship‐in‐a‐bottle biochip Laser & Photonics Reviews. ,vol. 8, pp. 458- 467 ,(2014) , 10.1002/LPOR.201400005
A. E. Geissberger, F. L. Galeener, Raman studies of vitreous Si O 2 versus fictive temperature Physical Review B. ,vol. 28, pp. 3266- 3271 ,(1983) , 10.1103/PHYSREVB.28.3266
Yves Bellouard, On the bending strength of fused silica flexures fabricated by ultrafast lasers [Invited] Optical Materials Express. ,vol. 1, pp. 816- 831 ,(2011) , 10.1364/OME.1.000816
Bo Lenssen, Yves Bellouard, Optically transparent glass micro-actuator fabricated by femtosecond laser exposure and chemical etching Applied Physics Letters. ,vol. 101, pp. 103503- ,(2012) , 10.1063/1.4750236
D. Homoelle, S. Wielandy, Alexander L. Gaeta, N. F. Borrelli, Charlene Smith, Infrared photosensitivity in silica glasses exposed to femtosecond laser pulses Optics Letters. ,vol. 24, pp. 1311- 1313 ,(1999) , 10.1364/OL.24.001311
Yves Bellouard, Ali Said, Mark Dugan, Philippe Bado, Fabrication of high-aspect ratio, micro-fluidic channels and tunnels using femtosecond laser pulses and chemical etching Optics Express. ,vol. 12, pp. 2120- 2129 ,(2004) , 10.1364/OPEX.12.002120
S. Juodkazis, K. Yamasaki, V. Mizeikis, S. Matsuo, H. Misawa, Formation of embedded patterns in glasses using femtosecond irradiation Applied Physics A. ,vol. 79, pp. 1549- 1553 ,(2004) , 10.1007/S00339-004-2845-1
Rozenn Le Parc, Claire Levelut, Jacques Pelous, Valérie Martinez, Bernard Champagnon, None, Influence of fictive temperature and composition of silica glass on anomalous elastic behaviour Journal of Physics: Condensed Matter. ,vol. 18, pp. 7507- 7527 ,(2006) , 10.1088/0953-8984/18/32/001
A. A. Griffith, The Phenomena of Rupture and Flow in Solids Philosophical Transactions of the Royal Society A. ,vol. 221, pp. 163- 198 ,(1921) , 10.1098/RSTA.1921.0006
Anand Agarwal, Minoru Tomozawa, Correlation of silica glass properties with the infrared spectra Journal of Non-crystalline Solids. ,vol. 209, pp. 166- 174 ,(1997) , 10.1016/S0022-3093(96)00542-X