In Situ X-ray Diffraction Study of the Phase Transition of Nanocrystalline In(OH)3 to In2O3

作者: Hongliang Zhu , Naiyan Wang , Lina Wang , Kuihong Yao , Xiaofei Shen

DOI: 10.1007/S10789-005-0178-X

关键词: X-ray crystallographyNuclear chemistryIndiumHydrothermal circulationOxideMaterials scienceTransmission electron microscopyCrystallographyPhase transitionNanocrystalline materialHydroxide

摘要: Single-crystalline indium oxide (In2O3) nanocubes were successfully prepared via dehydration of hydroxide (In(OH)3) synthesized by a hydrothermal method. In situ x-ray diffraction patterns the phase transition obtained. Transmission electron microscopy indicated that morphology In2O3 nanocrystallites was same as their precursors, In(OH)3 nanocrystallites. The reported method, shows simple and effective synthesis route for nanostructured materials.

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