New Perspectives in Monitoring the Flame Synthesis of Iron Oxide Nanoparticles: Addressing Solid and Gas-Phase Diagnostics Challenges
作者： Igor Rahinov , Marina Poliak , Alexey Fomin , Vladimir Tsionsky , Sergey Cheskis
DOI: 10.1557/OPL.2015.337
关键词: Materials science 、 Quartz crystal microbalance 、 Laser 、 Crystal 、 Iron oxide nanoparticles 、 Absorption spectroscopy 、 Particle 、 Spectrometer 、 Nanoparticle 、 Nanotechnology
摘要: Several techniques for in-situ monitoring and characterization of flame synthesized nanoparticles are described with the goal gaining further insight into mechanisms governing nanoparticle (NP) formation in reactors. These include: a combined particle mass spectrometer - quartz crystal microbalance apparatus (PMS-QCM); The Light Induced Detuning–Quartz Crystal Microbalance (LID-QCM) method; Application Intra Cavity Laser Absorption Spectroscopy (ICLAS) gas phase intermediates laden environment.
springer.com
sci-hub.se 参考文章(10)
I. Wlokas, A. Faccinetto, B. Tribalet, C. Schulz, A. Kempf, Mechanism of Iron Oxide Formation from Iron Pentacarbonyl‐Doped Low‐Pressure Hydrogen/Oxygen Flames International Journal of Chemical Kinetics. ,vol. 45, pp. 487- 498 ,(2013) , 10.1002/KIN.20786
Alexey Fomin, Marina Poliak, Vladimir Tsionsky, Sergey Cheskis, Igor Rahinov, A method for nanoparticle characterization by laser induced detuning of quartz crystal microbalance (LID-QCM) Sensors and Actuators B-chemical. ,vol. 202, pp. 861- 865 ,(2014) , 10.1016/J.SNB.2014.05.085
Alexey Fomin, Marina Poliak, Igor Rahinov, Vladimir Tsionsky, Sergey Cheskis, Combined particle mass spectrometer – Quartz crystal microbalance apparatus for in situ nanoparticle monitoring during flame assisted synthesis Combustion and Flame. ,vol. 160, pp. 2131- 2140 ,(2013) , 10.1016/J.COMBUSTFLAME.2013.04.011
Yogendra K. Mishra, Sören Kaps, Arnim Schuchardt, Ingo Paulowicz, Xin Jin, Dawit Gedamu, Stefan Freitag, Maria Claus, Sebastian Wille, Alexander Kovalev, Stanislav N. Gorb, Rainer Adelung, Fabrication of Macroscopically Flexible and Highly Porous 3D Semiconductor Networks from Interpenetrating Nanostructures by a Simple Flame Transport Approach Particle & Particle Systems Characterization. ,vol. 30, pp. 775- 783 ,(2013) , 10.1002/PPSC.201300197
Igor Rahinov, Alexey Fomin, Marina Poliak, Sergey Cheskis, Absorption electronic spectrum of gaseous FeO: in situ detection with intracavity laser absorption spectroscopy in a nanoparticle-generating flame reactor Applied Physics B. ,vol. 117, pp. 317- 323 ,(2014) , 10.1007/S00340-014-5838-6
A. Goldman, S. Cheskis, Intracavity laser absorption spectroscopy of sooting acetylene/air flames Applied Physics B. ,vol. 92, pp. 281- 286 ,(2008) , 10.1007/S00340-008-3084-5
An-Hui Lu, E. L. Salabas, Ferdi Schüth, Magnetic nanoparticles: Synthesis, protection, functionalization, and application Angewandte Chemie. ,vol. 46, pp. 1222- 1244 ,(2007) , 10.1002/ANIE.200602866
C. Janzen, P. Roth, Formation and characteristics of Fe2O3 nano-particles in doped low pressure H2/O2/Ar flames Combustion and Flame. ,vol. 125, pp. 1150- 1161 ,(2001) , 10.1016/S0010-2180(01)00235-8
Marina Poliak, Alexey Fomin, Vladimir Tsionsky, Sergey Cheskis, Irenaeus Wlokas, Igor Rahinov, On the mechanism of nanoparticle formation in a flame doped by iron pentacarbonyl Physical Chemistry Chemical Physics. ,vol. 17, pp. 680- 685 ,(2015) , 10.1039/C4CP04454A
Reto Strobel, Sotiris E. Pratsinis, Flame aerosol synthesis of smart nanostructured materials Journal of Materials Chemistry. ,vol. 17, pp. 4743- 4756 ,(2007) , 10.1039/B711652G