A New Generation of Self-etching Adhesives: Comparison with Traditional Acid Etch Technique

作者: Marcus Holzmeier , Martin Schaubmayr , Walter Dasch , Ursula Hirschfelder

DOI: 10.1007/S00056-008-0709-6

关键词: AdhesiveMaterials scienceScanning electron microscopeEnamel paintEtching (microfabrication)MineralogyDental bondingShear strengthBracketComposite materialPhosphoric acid

摘要: The aim of this study was to determine the shear bond strength (SBS), etching pattern and depth, debonding performance several market-leading, self-etching (SE) adhesives primarily used in restorative dentistry (iBond™, Clearfil™ S3 Bond, Protect AdheSE®, Xeno®III), two experimental (exp. Bond 1, exp. 2) one cement (SE Zement) with without prior phosphoric acid-etching, compare them an orthodontic product (Transbond™ Plus SE Primer) traditional acid-etch technique XT Primer, acid) All were applied on pumiced embedded bovine incisors following manufacturers' instructions. Then bracket each (coated Transbond™ composite) bonded (n = 20). polymerized for 20 s from incisal gingival sides using a halogen device positioned at constant 5 mm 45° angle specimen. specimens stored distilled water 24 h 37 °C before measuring SBS. ARI (adhesive remnant index) all determined sheared-off brackets each. After conditioning, surface texture morphologically evaluated scanning electron microscope (SEM) images, while depth confocal laserscanning (CLSM). groups tested normal distribution analyzed by applying ANOVA, Kruskal-Wallis or t test. In addition, Bonferroni correction used. median values SBS tests were: Zement 3.0 MPa, preceded acid 11.2 1: 7.4 2: 5.6 iBond™ 8.1 14.1 16.6 15.9 AdheSE® 16.0 Xeno®III 16.1 Primer 20.7 acidetching+ 21.0 MPa. With exception iBond™, we observed no significant differences among selfetching Restorative Dentistry comparison Primer. No apparent even when compared after acid-etching. Both bonding agents performed significantly worse than products mentioned above, failing demonstrate sufficient adhesive strength. SEM examination revealed less distinctive enamel-etching patterns CLSM analysis depths between 0.5 μm depending product. When used, residual composite remained enamel are suitable reduce risk fracture minimizing which turns means conditioning-related loss. More development is needed improve both Zement.

参考文章(35)
David H Pashley, Franklin R Tay, Aggressiveness of contemporary self-etching adhesives Dental Materials. ,vol. 17, pp. 430- 444 ,(2001) , 10.1016/S0109-5641(00)00104-4
Paul Lambrechts, Guido Vanherle, Jorge Perdigão, Jorge Leitão, Luís Lopes, Bart Van Meerbeek, Effects of a self-etching primer on enamel shear bond strengths and SEM morphology. American Journal of Dentistry. ,vol. 10, pp. 141- 146 ,(1997)
Franklin R Tay, David H Pashley, Aggressiveness of contemporary self-etching systems Dental Materials. ,vol. 17, pp. 296- 308 ,(2001) , 10.1016/S0109-5641(00)00087-7
Uno S, Finger Wj, Effect of acid etchant composition and etch duration on enamel loss and resin composite bonding American Journal of Dentistry. ,vol. 8, pp. 165- 169 ,(1995)
Pantelis Andreou, Corey A Felix, Richard B T Price, Lars Ehrnford, Comparison of quartz-tungsten-halogen, light-emitting diode, and plasma arc curing lights. Journal of Adhesive Dentistry. ,vol. 5, pp. 193- 207 ,(2003)
Gabriela Ibarra, Marcos A Vargas, Steve R Armstrong, Deborah S Cobbb, Microtensile bond strength of self-etching adhesives to ground and unground enamel. Journal of Adhesive Dentistry. ,vol. 4, pp. 115- 124 ,(2002)
Marcus Holzmeier, Claus-Peter Ernst, Brita Willershausen, Ursula Hirschfelder, In-vitro shear bond strength of self-etching versus traditional adhesives for orthodontic luting. Journal of Orofacial Orthopedics-fortschritte Der Kieferorthopadie. ,vol. 67, pp. 244- 259 ,(2006) , 10.1007/S00056-006-0546-4
L.R. Legler, D.H. Retief, E.L. Bradley, F.R. Denys, P.L. Sadowsky, Effects of phosphoric acid concentration and etch duration on the shear bond strength of an orthodontic bonding resin to enamel American Journal of Orthodontics and Dentofacial Orthopedics. ,vol. 96, pp. 485- 492 ,(1989) , 10.1016/0889-5406(89)90115-7
Adam W. Ostby, John J. Warren, Raed Ajlouni, Samir E. Bishara, John F. Laffoon, Early shear bond strength of a one-step self-adhesive on orthodontic brackets. Angle Orthodontist. ,vol. 76, pp. 689- 693 ,(2006) , 10.1043/0003-3219(2006)076[0689:ESBSOA]2.0.CO;2