Analysis of polynuclear aromatic hydrocarbons by glass capillary gas chromatography using simultaneous flame ionization and electron capture detection
作者： Alf Bjorseth , GÖRan Eklund
关键词: Analytical chemistry 、 Chemistry 、 Mass spectrometry 、 Capillary column 、 Capillary gas chromatography 、 Electron capture 、 Impurity 、 Flame ionization detector 、 Chromatography 、 Gas chromatography
摘要: The possibility of simultaneous application an electron capture (ECD) and a flame ionization detector (FID) connected to glass capillary column for analyzing polynuclear aromatic hydrocarbons (PNA) has been investigated. ECD/FID ratio is determined 46 PNA compounds. ratios vary from 0.02 117 with relative standard deviations better than 20 percent 10 replicate analyses. results suggest that the method may be used obtaining additional evidence in identifying environmental samples. Impurities transformation products were identified by computerized gas chromatography/mass spectrometry. Quinones diones are responsible high EC-response some trace components standard. An shown particulates urban atmospheres.
sci-hub.se 参考文章(16)
Göran Eklund, Björn Josefsson, Alf Björseth, Determination of chlorinated and brominated lipophilic compounds in spent bleach liquors from a sulphite pulp mill Journal of Chromatography A. ,vol. 150, pp. 161- 169 ,(1978) , 10.1016/S0021-9673(01)92108-9
H.-J. Klimisch*, D. Amrosius, Trennung polyzyklisher aromatischer kohlenwasserstoffe durch hochdruckflössigkeitschromatographie Journal of Chromatography A. ,vol. 120, pp. 299- 305 ,(1976) , 10.1016/S0021-9673(76)80007-6
Walter. Giger, Christian. Schaffner, Determination of polycyclic aromatic hydrocarbons in the environment by glass capillary gas chromatography Analytical Chemistry. ,vol. 50, pp. 234- 249 ,(1978) , 10.1021/AC50024A020
K. Grob, The glass capillary column in gas chromatography. A tool and a technique Chromatographia. ,vol. 8, pp. 423- 433 ,(1975) , 10.1007/BF02267578
Walter. Giger, Max. Blumer, Polycyclic aromatic hydrocarbons in the environment: isolation and characterization by chromatography, visible, ultraviolet, and mass spectrometry. Analytical Chemistry. ,vol. 46, pp. 1663- 1671 ,(1974) , 10.1021/AC60348A036
G.E. Moore, R.S. Thomas, J.L. Monkman, The routine determination of polycyclic hydrocarbons in airborne pollutants. Journal of Chromatography A. ,vol. 26, pp. 456- 464 ,(1967) , 10.1016/S0021-9673(01)98903-4
T. Doran, N. G. McTaggart, The Combined Use of High Efficiency Liquid and Capillary Gas Chromatography for the Determination of Polycyclic Aromatic Hydrocarbons in Automotive Exhaust Condensates and Other Hydrocarbon Mixtures Journal of Chromatographic Science. ,vol. 12, pp. 715- 721 ,(1974) , 10.1093/CHROMSCI/12.11.715
The determination of polynuclear aromatic hydrocarbons by gas-liquid chromatography. Annals of Occupational Hygiene. ,vol. 18, pp. 199- 206 ,(1975) , 10.1093/ANNHYG/18.3.199
D. A. Lane, H. K. Moe, Morris. Katz, Analysis of polynuclear aromatic hydrocarbons, some heterocyclics, and aliphatics with a single gas chromatograph column. Analytical Chemistry. ,vol. 45, pp. 1776- 1778 ,(1973) , 10.1021/AC60331A048
Alf Bjørseth, Analysis of polycyclic aromatic hydrocarbons in particulate matter by glass capillary gas chromatography Analytica Chimica Acta. ,vol. 94, pp. 21- 27 ,(1977) , 10.1016/S0003-2670(01)83627-8