NMR of sedimented, fibrillized, silica-entrapped and microcrystalline (metallo)proteins.
作者： Enrico Ravera , Tobias Schubeis , Tommaso Martelli , Marco Fragai , Giacomo Parigi
DOI: 10.1016/J.JMR.2014.12.019
关键词: Crystallography 、 Solid-state nuclear magnetic resonance 、 Fluorine-19 NMR 、 Chemistry 、 Chemical engineering 、 Nuclear magnetic resonance crystallography 、 Microcrystalline
摘要: Resolution and sensitivity in solid state NMR (SSNMR) can rival the results achieved by solution NMR, even outperform them case of large systems. However, several factors affect spectral quality SSNMR samples, not all systems turn out to be equally amenable for this methodology. In review we attempt at analyzing causes variable behavior providing hints increase chances experimental success.
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