Process Intensification: Precipitation of Barium Sulfate Using a Spinning Disk Reactor

作者: L. M. Cafiero , G. Baffi , A. Chianese , R. J. J. Jachuck

DOI: 10.1021/IE010654W

关键词: Aqueous solutionParticle numberCrystallizationParticle-size distributionSodium sulfatePrecipitation (chemistry)SupersaturationAnalytical chemistryMineralogyRotational speedChemistry

摘要: In this work, the use of a spinning disk reactor as unit for reaction−precipitation process is investigated. An experimental study reported concerning precipitation barium sulfate from aqueous solutions at 25 °C on 0.5 m in diameter. At rotational speed higher than 900 rpm, spontaneous took place and crystals ∼0.7 μm size were produced. supersaturation ratio 2000, number generated comparable with those literature when T-mixer used, but case disk, much lower specific dispersed power required.

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