Characterization of AgI nanoparticles synthesized in a spinning disk reactor
作者： Hwai-Shen Liu , Yao-Hsuan Wang , Chih-Chan Li , Clifford Y. Tai
DOI: 10.1016/J.CEJ.2011.12.035
关键词:
摘要: Abstract The main theme of this research was to characterize silver iodide nanoparticles that were synthesized via a liquid–liquid reaction conducted in spinning disk reactor (SDR). Silver nitrate and potassium used as the reactants, protecting agent tested mainly polyvinylpyrrolidone (PVP). experiment carried out continuous mode by injecting two streams AgNO3 KI solution continuously onto surface generate uniform small AgI particles. effects several operating variables, including concentration concentration, rotation speed, on particle size product yield investigated. In addition, crystal morphology, habits, bonding particles characterized. Finally, transition point produced changing from α-phase β/γ-phase measured compared with commercial 1 μm mean size. A large decrease temperature achieved, i.e., 49.6 °C versus 140.0 °C.
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