Optimization of Chitoasn Extract from Cockle Shell using Response Surface Methodology (RSM)
作者： Noorul Fhadila K , Ri Hanum Y S , Rahmah M , Zainal S
DOI:
关键词: Chitosan 、 Chemistry 、 Cockle 、 Shell (structure) 、 Yield (chemistry) 、 Anadara granosa 、 Chromatography 、 Central composite design 、 Response surface methodology 、 Extraction (chemistry)
摘要: This study was conducted to determine the optimum condition for extraction of chitosan by using response surface methodology (RSM). The extracted from cockle shell (Anadara granosa). optimized five levels and variables such as concentrations HCl (%), its immersion time (hr), concentration of NaOH (N), deacetylation temperature ( o C) (hr). process involved three main steps which were, dimineralization, deproteination deacetylation. A full factorial central composite design MINITAB software version 15 employed optimize yield chitosan. predicted at 8% with 16.5 hours immersion, 2.6N, 61 C, 1.5 hours time. determination coefficient R 2 = 95.4 also high, means experimental data acceptable.
ajouronline.com参考文章(19)
S.M. Cho, Y.S. Gu, S.B. Kim, Extracting optimization and physical properties of yellowfin tuna (Thunnus albacares) skin gelatin compared to mammalian gelatins Food Hydrocolloids. ,vol. 19, pp. 221- 229 ,(2005) , 10.1016/J.FOODHYD.2004.05.005
Manuela Taccari, Laura Canonico, Francesca Comitini, Ilaria Mannazzu, Maurizio Ciani, Screening of yeasts for growth on crude glycerol and optimization of biomass production. Bioresource Technology. ,vol. 110, pp. 488- 495 ,(2012) , 10.1016/J.BIORTECH.2012.01.109
R.V Muralidhar, R.R Chirumamila, R Marchant, P Nigam, A response surface approach for the comparison of lipase production by Candida cylindracea using two different carbon sources Biochemical Engineering Journal. ,vol. 9, pp. 17- 23 ,(2001) , 10.1016/S1369-703X(01)00117-6
Keisuke Kurita, Chitin and Chitosan: Functional Biopolymers from Marine Crustaceans Marine Biotechnology. ,vol. 8, pp. 203- 226 ,(2006) , 10.1007/S10126-005-0097-5
Kui Zhong, Qiang Wang, Optimization of ultrasonic extraction of polysaccharides from dried longan pulp using response surface methodology. Carbohydrate Polymers. ,vol. 80, pp. 19- 25 ,(2010) , 10.1016/J.CARBPOL.2009.10.066
Hamed Mirhosseini, Chin Ping Tan, Nazimah S.A. Hamid, Salmah Yusof, Boo Huey Chern, Characterization of the influence of main emulsion components on the physicochemical properties of orange beverage emulsion using response surface methodology Food Hydrocolloids. ,vol. 23, pp. 271- 280 ,(2009) , 10.1016/J.FOODHYD.2008.02.007
H.K Kim, J.G Kim, J.D Cho, J.W Hong, Optimization and characterization of UV-curable adhesives for optical communications by response surface methodology Polymer Testing. ,vol. 22, pp. 899- 906 ,(2003) , 10.1016/S0142-9418(03)00038-2
V. Jaikumar, V. Ramamurthi, Statistical analysis and optimization of acid dye biosorption by brewery waste biomass using response surface methodology. Modern Applied Science. ,vol. 3, pp. 71- 84 ,(2009) , 10.5539/MAS.V3N4P71
M Gopal, K Pakshirajan, T Swaminathan, Heavy metal removal by biosorption using Phanerochaete chrysosporium Applied Biochemistry and Biotechnology. ,vol. 102, pp. 227- 237 ,(2002) , 10.1385/ABAB:102-103:1-6:227
Md. Altaf, B.J. Naveena, M. Venkateshwar, E. Vijay Kumar, Gopal Reddy, Single step fermentation of starch to l(+) lactic acid by Lactobacillus amylophilus GV6 in SSF using inexpensive nitrogen sources to replace peptone and yeast extract – Optimization by RSM Process Biochemistry. ,vol. 41, pp. 465- 472 ,(2006) , 10.1016/J.PROCBIO.2005.07.011