Synthesis of mesoporous maghemite with high surface area and its adsorptive properties
作者： S. Asuha , Y.M. Zhao , S. Zhao , W. Deligeer
DOI: 10.1016/J.SOLIDSTATESCIENCES.2012.04.011
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摘要: Abstract Mesoporous maghemite (γ-Fe2O3) with high surface area was prepared by the thermal decomposition of Fe–urea complex ([Fe(CON2H4)6](NO3)3) aid cetyltrimethyl ammonium bromide (CTAB), and its adsorption ability for removal fluoride investigated. X-ray diffraction (XRD), nitrogen adsorption–desorption measurements, transmission electron micrograph (TEM) observations, magnetic measurements show that γ-Fe2O3 has a mesoporous structure crystallite size, specific area, properties can be controlled varying content CTAB in [Fe(CON2H4)6](NO3)3. The maximum capacity is estimated to 7.9 mg/g, which suggests an excellent adsorbent fluoride.
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F. J. KINGSTON, A. M. POSNER, J. P. QUIRK, ANION ADSORPTION BY GOETHITE AND GIBBSITE European Journal of Soil Science. ,vol. 23, pp. 177- 192 ,(1972) , 10.1111/J.1365-2389.1972.TB01652.X
Koon Fung Lam, King Lun Yeung, Gordon Mckay, Selective mesoporous adsorbents for Cr2O72- and Cu2+ separation Microporous and Mesoporous Materials. ,vol. 100, pp. 191- 201 ,(2007) , 10.1016/J.MICROMESO.2006.10.037
Shourong Wan, Junsheng Huang, Husheng Yan, Keliang Liu, Size-controlled preparation of magnetite nanoparticles in the presence of graft copolymers Journal of Materials Chemistry. ,vol. 16, pp. 298- 303 ,(2006) , 10.1039/B512605C
Koon Fung Lam, King Lun Yeung, Gordon McKay, A rational approach in the design of selective mesoporous adsorbents. Langmuir. ,vol. 22, pp. 9632- 9641 ,(2006) , 10.1021/LA061410P
Darko Makovec, Aljoša Košak, Andrej Žnidaršič, Miha Drofenik, The synthesis of spinel–ferrite nanoparticles using precipitation in microemulsions for ferrofluid applications Journal of Magnetism and Magnetic Materials. ,vol. 289, pp. 32- 35 ,(2005) , 10.1016/J.JMMM.2004.11.010
Feng Jiao, Jean-Claude Jumas, Manfred Womes, Alan V. Chadwick, Andrew Harrison, Peter G. Bruce, Synthesis of Ordered Mesoporous Fe3O4 and γ-Fe2O3 with Crystalline Walls Using Post-Template Reduction/Oxidation Journal of the American Chemical Society. ,vol. 128, pp. 12905- 12909 ,(2006) , 10.1021/JA063662I
Koon Fung Lam, King Lun Yeung, Gordon McKay, An investigation of gold adsorption from a binary mixture with selective mesoporous silica adsorbents. Journal of Physical Chemistry B. ,vol. 110, pp. 2187- 2194 ,(2006) , 10.1021/JP055577N
Qijie Guo, Xiaowei Teng, Saifur Rahman, Hong Yang, Patterned langmuir-blodgett films of monodisperse nanoparticles of iron oxide using soft lithography. Journal of the American Chemical Society. ,vol. 125, pp. 630- 631 ,(2003) , 10.1021/JA0275764
K. S. W. Sing, Reporting physisorption data for gas/solid systems with special reference to the determination of surface area and porosity (Recommendations 1984) Pure and Applied Chemistry. ,vol. 57, pp. 603- 619 ,(1985) , 10.1351/PAC198557040603
E. Tchomgui-Kamga, E. Ngameni, A. Darchen, Evaluation of removal efficiency of fluoride from aqueous solution using new charcoals that contain calcium compounds. joint international conference on information sciences. ,vol. 346, pp. 494- 499 ,(2010) , 10.1016/J.JCIS.2010.01.088