Versatile Cryostated Optically Transparent Thin-Layer Electrochemical (OTTLE) Cell for Variable-Temperature UV-Vis/IR Spectroelectrochemical Studies:
作者： F. Hartl , H. Luyten , H. A. Nieuwenhuis , G. C. Schoemaker
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摘要: … ESR spectroscopy at room temperature has revealed 25 that the oxidized solution in dry CH2C12 contained [Mn(CO)4(DBSQ… of [Mn(CO)3(DBSQ)] to give [Mn(CO)4(DBSQ)] and the …
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M. Krejčik, M. Daněk, F. Hartl, Simple construction of an infrared optically transparent thin-layer electrochemical cell: Applications to the redox reactions of ferrocene, Mn2(CO)10 and Mn(CO)3(3,5-di-t-butyl-catecholate)− Journal of Electroanalytical Chemistry. ,vol. 317, pp. 179- 187 ,(1991) , 10.1016/0022-0728(91)85012-E
X. H. Mu, Karl M. Kadish, Applications of thin-layer FTIR, UV-vis, and ESR spectroelectrochemistry for evaluating carbonyltetraphenylporphyrinruthenium redox reactions in nonaqueous media Langmuir. ,vol. 6, pp. 51- 56 ,(1990) , 10.1021/LA00091A008
Thomas P. DeAngelis, William R. Heineman, An electrochemical experiment using an optically transparent thin layer electrode Journal of Chemical Education. ,vol. 53, pp. 594- ,(1976) , 10.1021/ED053P594
Frantisek Hartl, Antonin Vlcek, Rhenium(I) carbonyl dioxolene complexes: electrochemical and spectroelectrochemical (resonance Raman, UV-visible and IR) study of [Re(CO)3L(Diox)]z and [Re(CO)2(PPh3)2(Diox)]z (L = Co, PPh3, P-dppe, THF, Ph3PO, Me2Co, py; z = -1, 0, +1) redox series Inorganic Chemistry. ,vol. 31, pp. 2869- 2876 ,(1992) , 10.1021/IC00039A037
W. Andrew. Nevin, A. B. P. Lever, Re-Usable Thin-Layer Spectroelectrochemical Cell for Non-Aqueous Solvent Systems. Analytical Chemistry. ,vol. 60, pp. 727- 730 ,(1988) , 10.1021/AC00158A028
R. R. Andréa, H. Luyten, M. A. Vuurman, D. J. Stufkens, A. Oskam, A Cryogenic Cell for Liquid Noble Gases. Vibrational Spectroscopy and Photochemistry of Transition Metal Carbonyls in Liquid Xenon Applied Spectroscopy. ,vol. 40, pp. 1184- 1190 ,(1986) , 10.1366/0003702864507684
John P. Bullock, David C. Boyd, Kent R. Mann, In situ infrared spectroelectrochemistry studies of ferrocene, [Rh2(dimen)2(dppm)2](PF6)2 and (mes)Cr(CO)3 (dimen = 1,8-diisocyanomenthane; dppm = bis(diphenylphosphino)methane); mes = mesitylene). A useful technique for the characterization of electrochemically generated organometallic species Inorganic Chemistry. ,vol. 26, pp. 3084- 3086 ,(1987) , 10.1021/IC00266A004
Graham A. Heath, Raphael G. Raptis, Low-temperature voltammetric study of rhenium isothiocyanate (Bu4N)2[Re2(NCS)8]. Spectroelectrochemical characterization of 9-electron [Re2(NCS)8]3- and 7-electron [Re2(NCS)8]1- and [Re2Cl8]1- Journal of the American Chemical Society. ,vol. 115, pp. 3768- 3769 ,(1993) , 10.1021/JA00062A050
David J. Curran, Philip B. Graham, Marvin D. Rausch, Infrared spectroelectrochemical observation of the reduction of iron pentacarbonyl Organometallics. ,vol. 12, pp. 2380- 2382 ,(1993) , 10.1021/OM00030A058
Michael J. Weaver, Richard A. Walton, Brian J. Brisdon, Starla K. Enger, Infrared spectroelectrochemistry of .eta.3-allyl dicarbonyl complexes of molybdenum(II) and tungsten(II) Inorganic Chemistry. ,vol. 26, pp. 3340- 3344 ,(1987) , 10.1021/IC00267A025