A polyvinyl alcohol-functionalized sorbent for extraction and determination of aminoglycoside antibiotics in honey

作者: Yuan Wang , Shunli Ji , Feng Zhang , Feifang Zhang , Bingcheng Yang

DOI: 10.1016/J.CHROMA.2015.05.032

关键词:

摘要: Abstract A novel highly hydrophilic sorbent simply prepared by coating polyvinyl alcohol (PVA) onto silica gel was used for extraction and determination of aminoglycoside antibiotics (AAs). The fabricated PVA is aimed to effectively protect core inside offers good property. In combination interaction chromatography tandem mass spectrometry, the performance evaluated selecting four model AAs (dihydrostreptomycin, streptomycin, kanamycin, spectinomycin). found have effective adsorption ability AAs, which superior or comparable those commercial ones. Good recoveries (84–112%) spiked in honey were obtained with precision (

参考文章(12)
Shunli Ji, Feifang Zhang, Xi Luo, Bingcheng Yang, Gaowa Jin, Jingyu Yan, Xinmiao Liang, Synthesis of molecularly imprinted polymer sorbents and application for the determination of aminoglycosides antibiotics in honey Journal of Chromatography A. ,vol. 1313, pp. 113- 118 ,(2013) , 10.1016/J.CHROMA.2013.08.072
Zonghui Yuan, Yanfei Tao, Dongmei Chen, Huan Yu, Lingli Huang, Zhaoying Liu, Xiaoqin Cao, Caixia Yan, Yuanhu Pan, Zhenli Liu, Simultaneous determination of 15 aminoglycoside(s) residues in animal derived foods by automated solid-phase extraction and liquid chromatography-tandem mass spectrometry. Food Chemistry. ,vol. 135, pp. 676- 683 ,(2012) , 10.1016/J.FOODCHEM.2012.04.086
Aikaterini M. Gremilogianni, Nikolaos C. Megoulas, Michael A. Koupparis, Hydrophilic interaction vs ion pair liquid chromatography for the determination of streptomycin and dihydrostreptomycin residues in milk based on mass spectrometric detection Journal of Chromatography A. ,vol. 1217, pp. 6646- 6651 ,(2010) , 10.1016/J.CHROMA.2010.04.059
Sara Bogialli, Roberta Curini, Antonio Di Corcia, Aldo Laganà, Monica Mele, Manuela Nazzari, Simple confirmatory assay for analyzing residues of aminoglycoside antibiotics in bovine milk: hot water extraction followed by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A. ,vol. 1067, pp. 93- 100 ,(2005) , 10.1016/J.CHROMA.2004.10.033
R. Oertel, W. Kirch, V. Neumeister, Hydrophilic interaction chromatography combined with tandem-mass spectrometry to determine six aminoglycosides in serum Journal of Chromatography A. ,vol. 1058, pp. 197- 201 ,(2004) , 10.1016/J.CHROMA.2004.08.158
Steven J. Lehotay, Katerina Mastovska, Alan R. Lightfield, Alberto Nuñez, Terry Dutko, Chilton Ng, Louis Bluhm, Rapid analysis of aminoglycoside antibiotics in bovine tissues using disposable pipette extraction and ultrahigh performance liquid chromatography-tandem mass spectrometry. Journal of Chromatography A. ,vol. 1313, pp. 103- 112 ,(2013) , 10.1016/J.CHROMA.2013.08.103
David N. Heller, James O. Peggins, Cristina B. Nochetto, Michelle L. Smith, O. Alberto Chiesa, Keesla Moulton, LC/MS/MS measurement of gentamicin in bovine plasma, urine, milk, and biopsy samples taken from kidneys of standing animals. Journal of Chromatography B. ,vol. 821, pp. 22- 30 ,(2005) , 10.1016/J.JCHROMB.2005.04.015