Precision Crystallization: Theory and Practice of Controlling Crystal Size
作者： Ingo H. Leubner
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摘要: Prior Models for Nucleation and Growth The Primitive Model Total Crystal Number Classical (Becker-Doering) Derivation of the Klein-Moisar Kharitanova Rate Maximum Balanced BNG Phase Assumptions Modeling Calculations Preliminary Considerations: Size Distribution Reaction Parameters Results Discussion Analytical Formation (Nucleation) under Kinetically Diffusion-Controlled Conditions Controlled Experiment: Theory Variables, Constants, Predictions Modeling: Separation Variables R, Cs, T Addition Solubility Temperature, Supersizing with Ripeners in Presence Ostwald Ripening Agents: Silver Bromide a Di-Thia Crown Ether as an Agent AgClBr (15:85) Ammonia AgBrI (97.4:2.6) 1,8-dihydroxy-3,6-dithiaoctane Nanosizing Restrainers Renucleation Growth, Renucleation, Rate: Experiments Continuous Crystallization Mixed-Suspension, Mixed-Product-Removal (MSMPR), or Stirred Tank Reactor (CSTR) Crystallizer Transient Behavior Precipitation Suspension A New Control Precipitations Seeded Epilogue Glossary Terms Bibliography Index
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