Unique trifurcated hydrogen bonding in a pseudopolymorph of tricyclohexane triperoxide (TCTP) and its thermal studies
作者： Chiranjeev Sharma Neupane , Satish Kumar Awasthi
DOI: 10.1016/J.TETLET.2012.08.134
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摘要: Abstract Tricyclohexane triperoxide (TCTP) was synthesized as a main by-product of tetraoxane synthesis and characterized by spectroscopic techniques viz. 1H NMR, 13C FT-IR Raman. The single crystal X-ray structure revealed the inclusion solvent in 1:1 stoichiometric ratio involving unique trifurcated C(sp3)–H⋯O hydrogen bonding imparting remarkable symmetry to molecule. thermal stability determined TG-DTA DSC.
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