Synthesis of 1-Thia-5,7-Diazacyclopenta[ cd ]- Phenalenes from 6(7)-Derivatives of Perimidine
作者： A. V. Aksenov , S. V. Shcherbakov , D. A. Lobach , N. N. Letichevskaya , E. A. Vasil’eva
DOI: 10.1007/S10593-014-1520-5
关键词:
摘要: Electrochemical oxidation of 6(7)-benzoylperimidines was shown to involve two stages single electron transfer. Based on cyclic voltammetry and microelectrolysis data, a synthetic method developed for the peri annelation thiophene ring benzoyl derivatives perimidine. A new proposed preparation 1-thia-5,7-diazacyclopenta[cd]phenalenes by fusing 6(7)-carbonyl perimidine with elemental sulfur.
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