Microwave‐Assisted Sample Preparation for Spectrochemistry

摘要: Microwave-assisted sample preparation was a major developmental step in combining the overall quality and speediness of spectrochemical analysis with initial converting solid samples into representative solutions. Instrumentation applications for organic inorganic are discussed detail after briefly addressing fundamentals method. The feasibility using diluted acid solutions pressurized oxygen vessels digestion is rationalized clearly related to recent advances reaction vessel materials interaction between matter microwave radiation. Applications based on microwave-induced combustion (MIC) procedures developed chemical speciation also highlighted. A list ideal attributes microwave-assisted proposed evaluated considering state art. Major needs, mainly capacity digesting large masses improvements throughput, pointed out.