Grain size evaluation of pulsed TiAlN nanocomposite coatings for cutting tools
作者： K. Bobzin , E. Lugscheider , M. Maes , P. Immich , S. Bolz
DOI: 10.1016/J.TSF.2006.11.002
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摘要: Abstract Nowadays advanced TiAlN coatings enable high performance and speed cutting. A side from excellent coating adhesion at the cutting edges choice of material, a fine grained physical vapour deposition is enabler for these operations. Isotropy composition vital importance performance. On industrial scale equipment, (Ti–Al ratio), crystallite size orientation are altered by changing pulse energy, duty cycle cathode power. The synthesized then analyzed common thin film application oriented techniques, regarding grain its influence on properties. For determination size, two methods, Debye Scherrer Warren Averbach compared. Finally, determined using method transmission electron microscopy comparison reasons.
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E. Lugscheider, K. Bobzin, C. Piñero, F. Klocke, T. Massmann, Development of a superlattice (Ti, Hf, Cr)N coating for cold metal forming applications Surface & Coatings Technology. ,vol. 177, pp. 616- 622 ,(2004) , 10.1016/S0257-8972(03)00935-6
S. Vepřek, P. Nesládek, A. Niederhofer, F. Glatz, M. Jı́lek, M. Šı́ma, Recent progress in the superhard nanocrystalline composites : towards their industrialization and understanding of the origin of the superhardness Surface & Coatings Technology. ,vol. 108, pp. 138- 147 ,(1998) , 10.1016/S0257-8972(98)00618-5
H. Natter, R. Hempelmann, Nanocrystalline Copper by Pulsed Electrodeposition: The Effects of Organic Additives, Bath Temperature, and pH The Journal of Physical Chemistry. ,vol. 100, pp. 19525- 19532 ,(1996) , 10.1021/JP9617837
H. Natter, M. Schmelzer, M.-S Löffler, C. E. Krill, A. Fitch, R. Hempelmann, Grain-growth kinetics of nanocrystalline iron studied in situ by synchrotron real-time X-ray diffraction Journal of Physical Chemistry B. ,vol. 104, pp. 2467- 2476 ,(2000) , 10.1021/JP991622D
Z Ji, J.A Haynes, M.K Ferber, J.M Rigsbee, Metastable tetragonal zirconia formation and transformation in reactively sputter deposited zirconia coatings Surface & Coatings Technology. ,vol. 135, pp. 109- 117 ,(2001) , 10.1016/S0257-8972(00)00910-5
P.Eh. Hovsepian, D.B. Lewis, W.-D. Münz, Recent progress in large scale manufacturing of multilayer/superlattice hard coatings Surface & Coatings Technology. ,vol. 133, pp. 166- 175 ,(2000) , 10.1016/S0257-8972(00)00959-2
J. Musil, Hard and superhard nanocomposite coatings Surface and Coatings Technology. ,vol. 125, pp. 322- 330 ,(2000) , 10.1016/S0257-8972(99)00586-1
S. A. Howard, R. L. Snyder, The use of direct convolution products in profile and pattern fitting algorithms. I. Development of algorithms Journal of Applied Crystallography. ,vol. 22, pp. 238- 243 ,(1989) , 10.1107/S0021889888014487
J. Musil, H. Hrubý, Superhard nanocomposite Ti1-xAlxN films prepared by magnetron sputtering Thin Solid Films. ,vol. 365, pp. 104- 109 ,(2000) , 10.1016/S0040-6090(00)00653-2
W.C. Oliver, G.M. Pharr, An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments Journal of Materials Research. ,vol. 7, pp. 1564- 1583 ,(1992) , 10.1557/JMR.1992.1564