Influence of electrical parameters on morphology of nanostructured TiO2 layers developed by electrochemical anodization

作者: Gabriela Strnad , Zoltan German-Sallo , Laszlo Jakab-Farkas , Cecilia Petrovan , Diana Portan

DOI: 10.1051/MATECCONF/201711204021

关键词:

摘要: Ti6Al4V alloy micro rough surfaces with TiO 2 self-organized nanostructured layers were synthesized using electrochemical anodization in phosphate/fluoride electrolyte, at different end potentials (5V, 10V, 15V, and 20 V). The current – time characteristics recorded, the link between evolution morphology of developing oxide was investigated. On flat we developed morphologies (random pores, nanopores 25…50 nm, highly organized nanotubes 50…100 nm diameter) depending on electrical parameters process. In our cell, optimized conditions, are able to superimpose (nanotubular or nanoporous) over structured titanium based materials used for biomedical implants.

参考文章(16)
Anca Mazare, Mirela Dilea, Daniela Ionita, Ioana Demetrescu, Electrochemical behavior in simulated body fluid of TiO2 nanotubes on TiAlNb alloy elaborated in various anodizing electrolyte Surface and Interface Analysis. ,vol. 46, pp. 186- 192 ,(2014) , 10.1002/SIA.5364
Poulomi Roy, Steffen Berger, Patrik Schmuki, TiO2 nanotubes: synthesis and applications. Angewandte Chemie. ,vol. 50, pp. 2904- 2939 ,(2011) , 10.1002/ANIE.201001374
Thomas J Webster, Ross, Anodizing color coded anodized Ti6Al4V medical devices for increasing bone cell functions. International Journal of Nanomedicine. ,vol. 8, pp. 109- 117 ,(2013) , 10.2147/IJN.S36203
Ernesto Beltrán-Partida, Aldo Moreno-Ulloa, Benjamín Valdez-Salas, Cristina Velasquillo, Monica Carrillo, Alan Escamilla, Ernesto Valdez, Francisco Villarreal, Improved Osteoblast and Chondrocyte Adhesion and Viability by Surface-Modified Ti6Al4V Alloy with Anodized TiO2 Nanotubes Using a Super-Oxidative Solution Materials. ,vol. 8, pp. 867- 883 ,(2015) , 10.3390/MA8030867
M Kulkarni, A Mazare, E Gongadze, Š Perutkova, V Kralj-Iglič, I Milošev, P Schmuki, A Iglič, M Mozetič, Titanium nanostructures for biomedical applications Nanotechnology. ,vol. 26, pp. 062002- ,(2015) , 10.1088/0957-4484/26/6/062002
Anca Mazare, Georgeta Totea, Cristian Burnei, Patrik Schmuki, Ioana Demetrescu, Daniela Ionita, Corrosion, antibacterial activity and haemocompatibility of TiO2 nanotubes as a function of their annealing temperature Corrosion Science. ,vol. 103, pp. 215- 222 ,(2016) , 10.1016/J.CORSCI.2015.11.021
Krunal Narendrakumar, Mukta Kulkarni, Owen Addison, Anca Mazare, Ita Junkar, Patrik Schmuki, Rachel Sammons, Aleš Iglič, Adherence of oral streptococci to nanostructured titanium surfaces. Dental Materials. ,vol. 31, pp. 1460- 1468 ,(2015) , 10.1016/J.DENTAL.2015.09.011
Karan Gulati, Abel Santos, David Findlay, Dusan Losic, Optimizing anodization conditions for the growth of titania nanotubes on curved surfaces Journal of Physical Chemistry C. ,vol. 119, pp. 16033- 16045 ,(2015) , 10.1021/ACS.JPCC.5B03383
Patrik Schmuki, Anca Mazare, Kiyoung Lee, One-dimensional titanium dioxide nanomaterials: nanotubes. Chemical Reviews. ,vol. 114, pp. 9385- 9454 ,(2014) , 10.1021/CR500061M