Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding.
作者： Kotaro Fujii , Ana Lazuen Garay , Janeen Hill , Elena Sbircea , Zhigang Pan
DOI: 10.1039/C0CC02635B
关键词:
摘要: Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal–organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance subjecting powder XRD data rigorous scrutiny in such applications is emphasized.
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