Mechanochemical synthesis: how grinding evolves.

作者: Kenneth D. M. Harris

DOI: 10.1038/NCHEM.1539

关键词: ChemistryChemical engineeringGrinding

摘要: An experimental set-up has been devised to monitor mechanochemical processes in situ, yielding direct insights into mechanistic and kinetic aspects of solid-state reactions that are promoted by grinding, such as the synthesis metal–organic frameworks.

参考文章(11)
V. V. Boldyrev, K. Tkáčová, Mechanochemistry of Solids: Past, Present, and Prospects Journal of Materials Synthesis and Processing. ,vol. 8, pp. 121- 132 ,(2000) , 10.1023/A:1011347706721
L. Takacs, The mechanochemical reduction of AgCl with metals Journal of Thermal Analysis and Calorimetry. ,vol. 90, pp. 81- 84 ,(2007) , 10.1007/S10973-007-8479-8
Kotaro Fujii, Ana Lazuen Garay, Janeen Hill, Elena Sbircea, Zhigang Pan, Mingcan Xu, David C. Apperley, Stuart L. James, Kenneth D. M. Harris, Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding. Chemical Communications. ,vol. 46, pp. 7572- 7574 ,(2010) , 10.1039/C0CC02635B
Eugene Y. Cheung, Simon J. Kitchin, Kenneth D. M. Harris, Yoshitane Imai, Nobuo Tajima, Reiko Kuroda, Direct structure determination of a multicomponent molecular crystal prepared by a solid-state grinding procedure. Journal of the American Chemical Society. ,vol. 125, pp. 14658- 14659 ,(2003) , 10.1021/JA030506S
H. M. Rietveld, A profile refinement method for nuclear and magnetic structures Journal of Applied Crystallography. ,vol. 2, pp. 65- 71 ,(1969) , 10.1107/S0021889869006558
Tomislav Friščić, Ernest Meštrović, Dijana Škalec Šamec, Branko Kaitner, László Fábián, None, One-Pot Mechanosynthesis with Three Levels of Molecular Self-Assembly: Coordination Bonds, Hydrogen Bonds and Host-Guest Inclusion Chemistry: A European Journal. ,vol. 15, pp. 12644- 12652 ,(2009) , 10.1002/CHEM.200901058
Tomislav Friščić, Ivan Halasz, Patrick J. Beldon, Ana M. Belenguer, Frank Adams, Simon A.J. Kimber, Veijo Honkimäki, Robert E. Dinnebier, Real-time and in situ monitoring of mechanochemical milling reactions Nature Chemistry. ,vol. 5, pp. 66- 73 ,(2013) , 10.1038/NCHEM.1505
Stuart L. James, Christopher J. Adams, Carsten Bolm, Dario Braga, Paul Collier, Tomislav Friščić, Fabrizia Grepioni, Kenneth D. M. Harris, Geoff Hyett, William Jones, Anke Krebs, James Mack, Lucia Maini, A. Guy Orpen, Ivan P. Parkin, William C. Shearouse, Jonathan W. Steed, Daniel C. Waddell, Mechanochemistry: opportunities for new and cleaner synthesis Chemical Society Reviews. ,vol. 41, pp. 413- 447 ,(2012) , 10.1039/C1CS15171A
Patrick J. Beldon, László Fábián, Robin S. Stein, A. Thirumurugan, Anthony K. Cheetham, Tomislav Friščić, Rapid Room‐Temperature Synthesis of Zeolitic Imidazolate Frameworks by Using Mechanochemistry Angewandte Chemie. ,vol. 49, pp. 9640- 9643 ,(2010) , 10.1002/ANIE.201005547
Jie-Peng Zhang, Yue-Biao Zhang, Jian-Bin Lin, Xiao-Ming Chen, Metal Azolate Frameworks: From Crystal Engineering to Functional Materials Chemical Reviews. ,vol. 112, pp. 1001- 1033 ,(2012) , 10.1021/CR200139G