Novel simplified absorption-catalytic method of sample preparation for AMS analysis designed at the Laboratory of Radiocarbon Methods of Analysis (LRMA) in Novosibirsk Akademgorodok

作者: A.I. Lysikov , P.N. Kalinkin , K.A. Sashkina , A.G. Okunev , E.V. Parkhomchuk

DOI: 10.1016/J.IJMS.2018.08.003

关键词:

摘要: Abstract A new absorption-catalytic method of sample preparation for AMS 14C analysis has been designed. The semi-automatic graphitization equipment consists catalytic combustion, selective absorption/desorption CO2 and zones. Sample combustion followed by separation takes less than 30 min that allows plenty samples to be processed in a short time. average conversion graphite turned out 75%. Achieved value background induced contamination with contemporary carbon is about 1.2 pMC. proposed reproducible according results the OX-I OX-II oxalic acid standards measured from 2015 2018 successfully used dating lake sediments. agree data other laboratories. penetration model aerosol particles inhaled at low dose mice studied means designed method.

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