Effect of synthesis temperature and aging on the microstructure and hardness of Ti-Zr-C
作者： Taoran Ma , Peter Hedström , Joakim Odqvist
DOI: 10.1016/J.IJRMHM.2018.02.001
关键词:
摘要: Abstract The mixed carbide Ti-Zr-C has been synthesized through carbothermal reduction of TiZrO4 at 2200 °C, 2300 °C, and 2400 °C. As-synthesized was subsequently aged 1400 °C to study phase separation. Microstructural investigations nano-indentation measurements were performed. It found that the synthesis temperature important for homogeneity porosity as-synthesized powder, which strongly influenced subsequent separation upon aging. occurred via discontinuous precipitation, high-angle boundaries preferred. Furthermore, characteristics precipitation in present system with a miscibility gap compared those classical precipitation. Finally, fully decomposed particles be slightly harder than unaged particles.
sci-hub.se 参考文章(28)
R. Monzen, Misorientation dependence of discontinuous precipitation in Cu-Be alloy bicrystals Journal of Materials Science. ,vol. 35, pp. 5839- 5843 ,(2000) , 10.1023/A:1026700222794
Electron Backscatter Diffraction in Materials Science Electron Backscatter Diffraction in Materials Science edited by Adam J. Schwartz. ,(2000) , 10.1007/978-0-387-88136-2
Masato Enomoto, Jong K. Lee, Hubert I. Aaronson, Mechanisms of Diffusional Phase Transformations in Metals and Alloys ,(2010)
S Hirth, G Gottstein, Misorientation effects on discontinuous precipitation in Al–Ag–Ga Acta Materialia. ,vol. 46, pp. 3975- 3984 ,(1998) , 10.1016/S1359-6454(98)00061-5
Hugo M. Ortner, Peter Ettmayer, Hans Kolaska, Ivi Smid, The history of the technological progress of hardmetals International Journal of Refractory Metals & Hard Materials. ,vol. 49, pp. 3- 8 ,(2014) , 10.1016/J.IJRMHM.2014.04.016
K.N Tu, D Turnbull, Morphology of cellular precipitation of tin from lead-tin bicrystals-ii Acta Metallurgica. ,vol. 15, pp. 369- 376 ,(1967) , 10.1016/0001-6160(67)90007-7
Pierre Hovington, Dominique Drouin, Raynald Gauvin, CASINO: A new monte carlo code in C language for electron beam interaction —part I: Description of the program Scanning. ,vol. 19, pp. 1- 14 ,(2006) , 10.1002/SCA.4950190101
Alexandre Maitre, Pierre Lefort, Solid state reaction of zirconia with carbon Solid State Ionics. ,vol. 104, pp. 109- 122 ,(1997) , 10.1016/S0167-2738(97)00398-6
E. Hryha, P. Zubko, E. Dudrová, L. Pešek, S. Bengtsson, An application of universal hardness test to metal powder particles Journal of Materials Processing Technology. ,vol. 209, pp. 2377- 2385 ,(2009) , 10.1016/J.JMATPROTEC.2008.05.038
F.J.A Den Broeder, W.G Burgers, An x-ray diffraction study of the decomposition of tungsten-chromium solid solution Acta Metallurgica. ,vol. 16, pp. 265- 268 ,(1968) , 10.1016/0001-6160(68)90011-4