Measurement of Carbon Condensates Using Small-Angle X-ray Scattering During Detonation of High Explosives

作者: T. M. Willey , M. Bagge-Hansen , L. Lauderbach , R. Hodgin , D. Hansen

DOI: 10.1063/1.4971470

关键词:

摘要: The lack of experimental validation for processes occurring at sub-micron length scales on time ranging from nanoseconds to microseconds hinders detonation model development. Particularly, quantification late-time energy release requires measurement carbon condensation kinetics behind fronts. A new small-angle x-ray scattering (SAXS) endstation has been developed use Dynamic Compression Sector observe during detonation. and beamline demonstrate unprecedented fidelity; SAXS profiles can be acquired single pulses, which in 24-bunch mode are about 80 ps duration arrive every 153.4 ns. This paper presents both the current temporal capabilities this beamline, ability distinguish different condensate morphologies as they form To capabilities, three shots hexanitrostilbene (HNS) interleaved show evolution SAX...

参考文章(26)
J. A. Viecelli, S. Bastea, J. N. Glosli, F. H. Ree, Phase transformations of nanometer size carbon particles in shocked hydrocarbons and explosives The Journal of Chemical Physics. ,vol. 115, pp. 2730- 2736 ,(2001) , 10.1063/1.1386418
Gilbert Collins, David S Moore, Choong-Shik Yoo, William Buttler, Michael Furlanetto, William Evans, 18th APS-SCCM and 24th AIRAPT Journal of Physics: Conference Series. ,vol. 500, pp. 001002- ,(2014) , 10.1088/1742-6596/500/0/001002
O.V. Evdokov, M.G. Fedotov, G.N. Kulipanov, L.A. Luckjanchikov, N.Z. Lyakhov, S.I. Mishnev, M.R. Sharafutdinov, M.A. Sheromov, K.A. Ten, V.M. Titov, B.P. Tolochko, P.I. Zubkov, Dynamics of the formation of the condensed phase particles at detonation of high explosives Nuclear Instruments & Methods in Physics Research Section A-accelerators Spectrometers Detectors and Associated Equipment. ,vol. 470, pp. 236- 239 ,(2001) , 10.1016/S0168-9002(01)01057-9
E. R. Pruuel, K. A. Ten, B. P. Tolochko, L. A. Merzhievskii, L. A. Luk’yanchikov, V. M. Aul’chenko, V. V. Zhulanov, L. I. Shekhtman, V. M. Titov, Implementation of the capability of synchrotron radiation in a study of detonation processes Doklady Physics. ,vol. 58, pp. 24- 28 ,(2013) , 10.1134/S1028335813010035
Byron Freelon, Kamlesh Suthar, Jan Ilavsky, A multi‐length‐scale USAXS/SAXS facility: 10–50 keV small‐angle X‐ray scattering instrument Journal of Applied Crystallography. ,vol. 46, pp. 1508- 1512 ,(2013) , 10.1107/S0021889813021900
Y. M. Gupta, Stefan J. Turneaure, K. Perkins, K. Zimmerman, N. Arganbright, G. Shen, P. Chow, Real-time, high-resolution x-ray diffraction measurements on shocked crystals at a synchrotron facility Review of Scientific Instruments. ,vol. 83, pp. 123905- ,(2012) , 10.1063/1.4772577
Jan Ilavsky, Andrew J. Allen, Lyle E. Levine, Fan Zhang, Pete R. Jemian, Gabrielle G. Long, High‐energy ultra‐small‐angle X‐ray scattering instrument at the Advanced Photon Source Journal of Applied Crystallography. ,vol. 45, pp. 1318- 1320 ,(2012) , 10.1107/S0021889812040022
M. S. Shaw, J. D. Johnson, Carbon clustering in detonations Journal of Applied Physics. ,vol. 62, pp. 2080- 2085 ,(1987) , 10.1063/1.339554
M. Riad Manaa, Evan J. Reed, Laurence E. Fried, Nir Goldman, Nitrogen-rich heterocycles as reactivity retardants in shocked insensitive explosives. Journal of the American Chemical Society. ,vol. 131, pp. 5483- 5487 ,(2009) , 10.1021/JA808196E
J. A. Viecelli, F. H. Ree, Carbon particle phase transformation kinetics in detonation waves Journal of Applied Physics. ,vol. 88, pp. 683- 690 ,(2000) , 10.1063/1.373721