Quantitation of the active compound and major excipients in a pharmaceutical formulation by near infrared diffuse reflectance spectroscopy with fibre optical probe
作者： M. Blanco , J. Coello , H. Iturriaga , S. Maspoch , C. de la Pezuela
DOI: 10.1016/0003-2670(96)00250-4
关键词:
摘要: A new method for analyses of a commercial pharmaceutical formulation based on near infrared diffuse reflectance spectroscopy (NIRRS) with fibre optical probe and using partial least-squares regression (PLS) multivariate calibration is proposed. Analyses include the determination active compound major excipients. The influence spectral mode wavelength range used are studied. Satisfactory predictive results production samples require laboratory-made covering concentration involved in manufacturing process, as well from various batches, which introduce variation sources inherent such process. number to be order ensure correct prediction discussed.
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sci-hub.se 参考文章(14)
M. Blanco, J. Coello, H. Iturriaga, S. Maspoch, C. de la Pezuela, E. Russo, Control analysis of a pharmaceutical preparation by near-infrared reflectance spectroscopy. A comparative study of a spinning module and fibre optic probe Analytica Chimica Acta. ,vol. 298, pp. 183- 191 ,(1994) , 10.1016/0003-2670(94)00275-4
M. Blanco, J. Coello, H. Iturriaga, S. Maspoch, C. de la Pezuela, Determination of ascorbic acid in pharmaceutical preparations by near infrared reflectance spectroscopy Talanta. ,vol. 40, pp. 1671- 1676 ,(1993) , 10.1016/0039-9140(93)80083-4
Matthias. Otto, Wolfhard. Wegscheider, Spectrophotometric multicomponent analysis applied to trace metal determinations Analytical Chemistry. ,vol. 57, pp. 63- 69 ,(1985) , 10.1021/AC00279A020
Lorna S. Aucott, Paul H. Garthwaite, Stephen T. Buckland, Transformations to reduce the effect of particle size in near-infrared spectra Analyst. ,vol. 113, pp. 1849- 1854 ,(1988) , 10.1039/AN9881301849
David M. Haaland, Edward V. Thomas, Partial least-squares methods for spectral analyses. 1. Relation to other quantitative calibration methods and the extraction of qualitative information Analytical Chemistry. ,vol. 60, pp. 1193- 1202 ,(1988) , 10.1021/AC00162A020
J. L. Ilari, H. Martens, T. Isaksson, Determination of Particle Size in Powders by Scatter Correction in Diffuse Near-Infrared Reflectance Applied Spectroscopy. ,vol. 42, pp. 722- 728 ,(1988) , 10.1366/0003702884429058
P.A. Salamin, Y. Cornelis, H. Bartels, Identification of chemical substances by their near-infrared spectra Chemometrics and Intelligent Laboratory Systems. ,vol. 3, pp. 329- 333 ,(1988) , 10.1016/0169-7439(88)80032-7
W. Plugge, C. van der Vlies, Near-infrared spectroscopy as an alternative to assess compliance of ampicillin trihydrate with compendial specifications Journal of Pharmaceutical and Biomedical Analysis. ,vol. 11, pp. 435- 442 ,(1993) , 10.1016/0731-7085(93)80154-S
Emilw. Ciurczak, Uses of near-infrared spectroscopy in pharmaceutical analysis Applied Spectroscopy Reviews. ,vol. 23, pp. 147- 163 ,(1987) , 10.1080/05704928708060445
W. Plugge, C. van der Vliest, The use of near infrared spectroscopy in the quality control laboratory of the pharmaceutical industry Journal of Pharmaceutical and Biomedical Analysis. ,vol. 10, pp. 797- 803 ,(1992) , 10.1016/0731-7085(91)80083-L