作者: Masahiko Tanaka , Yoshio Katsuya , Akiji Yamamoto
DOI: 10.1063/1.2956972
关键词:
摘要: A new large radius imaging plate diffraction camera for high-resolution and high-throughput synchrotron x-ray powder by means of multiple exposures has been developed an insertion device beamline SPring-8, Japan. The consists a cylindrical shape cassette that is 400mm in length 954.9mm cylinder radius. designed to be mounted on the 2θ arm diffractometer BL15XU SPring-8. One covers 24° several times exposure changing 2θ-setting angle necessary obtain whole data up high region. pixel corresponds 0.003° when readout size 50μm squares. Separately collected are translated 2θ-intensity format connected comparing peak background intensity included overlapped area. time less than 120s most samples about 3min; thus, tot...