Nuclear overhauser effect and conformational states of cellobiose in aqueous solution
作者： Grigory M. Lipkind , Alexander S. Shashkov , Nikolay K. Kochetkov
DOI: 10.1016/S0008-6215(00)90451-8
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摘要: Abstract A nuclear Overhauser enhancement in α-cellobiose 1-phosphate, resulting from pre-irradiation of H-1′ the non-reducing glucosyl group, was measured and calculated theoretically. Comparison these data reveals a complicated conformational equilibrium aqueous solutions cellobiose derivative.
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sci-hub.se 参考文章(16)
Steen Melberg, Kjeld Rasmussen, Conformations of disaccharides by empirical force-field calculations: part II, β-cellobiose Carbohydrate Research. ,vol. 71, pp. 25- 34 ,(1979) , 10.1016/S0008-6215(00)86057-7
Roy A. Scott, Harold A. Scheraga, Conformational Analysis of Macromolecules. II. The Rotational Isomeric States of the Normal Hydrocarbons Journal of Chemical Physics. ,vol. 44, pp. 3054- 3069 ,(1966) , 10.1063/1.1727180
Grigory M. Lipkind, Valery E. Verovsky, Nikolay K. Kochetkov, Conformational states of cellobiose and maltose in solution: A comparison of calculated and experimental data Carbohydrate Research. ,vol. 133, pp. 1- 13 ,(1984) , 10.1016/0008-6215(84)85177-0
D.A. Rees, R.J. Skerrett, Conformational analysis of cellobiose, cellulose, and xylan Carbohydrate Research. ,vol. 7, pp. 334- 348 ,(1968) , 10.1016/S0008-6215(00)81206-9
Gerhard Wagner, Kurt Wuthrich, Truncated driven nuclear overhauser effect (TOE). A new technique for studies of selective 1H1H overhauser effects in the presence of spin diffusion Journal of Magnetic Resonance. ,vol. 33, pp. 675- 680 ,(1979) , 10.1016/0022-2364(79)90180-X
Henning Thøgersen, Raymond U. Lemieux, Klaus Bock, Bernd Meyer, Further justification for the exo-anomeric effect. Conformational analysis based on nuclear magnetic resonance spectroscopy of oligosaccharides Canadian Journal of Chemistry. ,vol. 60, pp. 44- 57 ,(1982) , 10.1139/V82-009
Gordon K. Hamer, Felipe Balza, Natsuko Cyr, Arthur S. Perlin, A conformational study of methyl β-cellobioside-d8 by 13C nuclear magnetic resonance spectroscopy: dihedral angle dependence of 3JC–H in 13C—O—C—1H arrays Canadian Journal of Chemistry. ,vol. 56, pp. 3109- 3116 ,(1978) , 10.1139/V78-508
Roger E. Schirmer, Joseph H. Noggle, Jeffrey Paul. Davis, Phillip A. Hart, Determination of molecular geometry by quantitative application of the nuclear Overhauser effect Journal of the American Chemical Society. ,vol. 92, pp. 3266- 3273 ,(1970) , 10.1021/JA00714A005
André De Bruyn, Marc Anteunis, Conformation of the C-5/C-6 fragment of aldohexopyranoses Carbohydrate Research. ,vol. 47, pp. 311- 314 ,(1976) , 10.1016/S0008-6215(00)84197-X
Michael L. Hayes, Anthony S. Serianni, Robert Barker, Methyl β-lactoside: 600-MHz 1H- and 75-MHz 13C-n.m.r. studies of 2H- and 13C-enriched compounds Carbohydrate Research. ,vol. 100, pp. 87- 101 ,(1982) , 10.1016/S0008-6215(00)81028-9