Construction and characterization of the fringe field monochromator for a field emission gun

作者: H.W Mook , P Kruit

DOI: 10.1016/S0304-3991(99)00193-X

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摘要: Abstract Although some microscopes have shown stabilities sufficient to attain below 0.1 eV spectral resolution in high-resolution electron energy loss spectroscopy, the intrinsic width of high brightness source (0.3–0.6 eV) has been limiting resolution. To lower 50 meV without unnecessary brightness, a monochromator designed consisting short (4 mm) fringe field Wien filter and 150 nm selection slit (nanoslit) both be incorporated gun area microscope. A prototype built tested an ultra-high-vacuum setup (10 −9  mbar). The monochromator, operating on Schottky emission gun, showed stable reproducible operation. nanoslits did not contaminate structure remained stable. By measuring current through direct image beam could attained aligned use Good dispersed imaging conditions were found indicating ultimate 55 meV. Mark II (FFM) was constructed compatible with cold tungsten emitter VG scanning transmission microscope at IBM T.J. Watson research center, New York. 100 kV distribution measured using displayed filtering capability. retarding spectrometer used show 61 meV EELS system FFM is which can This makes it directly applicable for microscopy low-voltage microscopy, where caused by chromatic blur spot.

参考文章(14)
H.W Mook, P Kruit, Optics and design of the fringe field monochromator for a Schottky field emission gun Nuclear Instruments & Methods in Physics Research Section A-accelerators Spectrometers Detectors and Associated Equipment. ,vol. 427, pp. 109- 120 ,(1999) , 10.1016/S0168-9002(98)01511-3
P. E. BATSON, NEAR-ATOMIC-RESOLUTION EELS IN SILICON-GERMANIUM ALLOYS Journal of Microscopy. ,vol. 180, pp. 204- 210 ,(1995) , 10.1111/J.1365-2818.1995.TB03679.X
Masami Thrauchi, Ryuichi Kuzuo, Futami Satoh, Michiyoshi Thnaka, Katsushige Tsuno, Junichi Ohyama, Performance of a new high-resolution electron energy-loss spectroscopy microscope Microscopy Microanalysis Microstructures. ,vol. 2, pp. 351- 358 ,(1991) , 10.1051/MMM:0199100202-3035100
P. E. Batson, High‐energy resolution electron spectrometer for 1‐nm spatial analysis Review of Scientific Instruments. ,vol. 57, pp. 43- 48 ,(1986) , 10.1063/1.1139116
Michel Troyon, Pulsed field emission electron or ion gun with energy filter Microelectronic Engineering. ,vol. 6, pp. 105- 110 ,(1987) , 10.1016/0167-9317(87)90023-2
H. Rose, Prospects for realizing a sub-Å sub-eV resolution EFTEM Ultramicroscopy. ,vol. 78, pp. 13- 25 ,(1999) , 10.1016/S0304-3991(99)00025-X
MJ Fransen, JS Faber, Th L Van Rooy, PC Tiemeijer, P Kruit, Experimental evaluation of the extended Schottky model for ZrO/W electron emission Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures. ,vol. 16, pp. 2063- 2072 ,(1998) , 10.1116/1.590128