Electrospinning Synthesis and Luminescence Properties of One-Dimensional Zn2SiO4:Mn2+ Microfibers and Microbelts
作者： Lili Wang , Xiaoming Liu , Zhiyao Hou , Chunxia Li , Piaoping Yang
DOI: 10.1021/JP806392A
关键词:
摘要: One-dimensional Mn2+-doped Zn2SiO4 microbelts and microfibers were prepared by a simple cost-effective electrospinning process. X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric differential thermal analysis (TG-DTA), scanning electron microscopy (SEM), energy-dispersive spectrum (EDS), transmission (TEM), high-resolution (HRTEM), photoluminescence (PL), cathodoluminescence (CL) spectra as well kinetic decays used to characterize the samples. The XRD DTA results show that phase begins crystallize at 800 °C crystallizes completely around 1000 °C. SEM indicate as-prepared microbelts/fibers are smooth, whose diameters decrease with increasing annealing temperature. average diameter of Zn2SiO4:Mn2+ annealed is 0.32 μm, their lengths reach up several millimeters. width thickness Zn2SiO4:M...
acs.org
irgrid.ac.cn参考文章(44)
Takeshi Ohgaki, Akihisa Higashida, Kohei Soga, Atsuo Yasumori, Eu-Doped CaAl2Si2O8 Nanocrystalline Phosphors Crystallized from the CaO – Al2O3 – SiO2 Glass System Journal of The Electrochemical Society. ,vol. 154, ,(2007) , 10.1149/1.2712834
Jiangtao Hu, Min Ouyang, Peidong Yang, Charles M. Lieber, Controlled growth and electrical properties of heterojunctions of carbon nanotubes and silicon nanowires Nature. ,vol. 399, pp. 48- 51 ,(1999) , 10.1038/19941
Jianhua Hao, J. Gao, Michael Cocivera, Green, blue, and yellow cathodoluminescence of Ba2B5O9Cl thin-films doped with Tb3+, Tm3+, and Mn2+ Applied Physics Letters. ,vol. 82, pp. 2224- 2226 ,(2003) , 10.1063/1.1565704
D. Y. Kong, M. Yu, C. K. Lin, X. M. Liu, J. Lin, J. Fang, Sol-gel Synthesis and Characterization of Zn2SiO4 : Mn@SiO2 Spherical Core-Shell Particles Journal of The Electrochemical Society. ,vol. 152, ,(2005) , 10.1149/1.1990612
Xiaoming Liu, Jun Lin, None, Nanocrystalline LaGaO3:Tm3+ as an efficient blue phosphor for field emission displays with high color purity Applied Physics Letters. ,vol. 90, pp. 184108- ,(2007) , 10.1063/1.2735556
M. Yu, J. Lin, J. Fang, Silica Spheres Coated with YVO4:Eu3+ Layers via Sol−Gel Process: A Simple Method To Obtain Spherical Core−Shell Phosphors Chemistry of Materials. ,vol. 17, pp. 1783- 1791 ,(2005) , 10.1021/CM0479537
Chunxia Li, Jun Yang, Piaoping Yang, Hongzhou Lian, Jun Lin, Hydrothermal Synthesis of Lanthanide Fluorides LnF3 (Ln = La to Lu) Nano-/Microcrystals with Multiform Structures and Morphologies Chemistry of Materials. ,vol. 20, pp. 4317- 4326 ,(2008) , 10.1021/CM800279H
Yiying Wu, Haoquan Yan, Michael Huang, Benjamin Messer, Jae Hee Song, Peidong Yang, Inorganic Semiconductor Nanowires: Rational Growth, Assembly, and Novel Properties Chemistry: A European Journal. ,vol. 8, pp. 1260- 1268 ,(2002) , 10.1002/1521-3765(20020315)8:6<1260::AID-CHEM1260>3.0.CO;2-Q
Travis J. Sill, Horst A. von Recum, Electrospinning: Applications in drug delivery and tissue engineering Biomaterials. ,vol. 29, pp. 1989- 2006 ,(2008) , 10.1016/J.BIOMATERIALS.2008.01.011
Ana Maria Pires, Marian Rosaly Davolos, Luminescence of Europium(III) and Manganese(II) in Barium and Zinc Orthosilicate Chemistry of Materials. ,vol. 13, pp. 21- 27 ,(2001) , 10.1021/CM000063G