Boric Acid / Glycerol as an Efficient Catalyst for Synthesis of Thiomorpholine 1,1-Dioxide by Double Michael Addition Reaction in Water
作者： Azim Ziyaei Halimehjnai , Seyedmorteza Hosseyni , Hadi Gholami , Mohammed M. Hashemi
DOI: 10.1080/00397911.2011.594930
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摘要: Abstract Thiomorpholine 1,1-dioxides were prepared with double Michael addition reaction of aromatic amines to divinyl sulfone catalyzed by boric acid / glycerol in water. This catalyst system was also used for the electron-deficient alkenes. The is simple and green gives good excellent yields.
sci-hub.se 参考文章(13)
Mihir K. Chaudhuri, Sahid Hussain, Boric acid catalyzed thia-Michael reactions in water or alcohols Journal of Molecular Catalysis A-chemical. ,vol. 269, pp. 214- 217 ,(2007) , 10.1016/J.MOLCATA.2007.01.014
Xin Ai, Xin Wang, Jin-ming Liu, Ze-mei Ge, Tie-ming Cheng, Run-tao Li, An effective aza-Michael addition of aromatic amines to electron-deficient alkenes in alkaline Al2O3 Tetrahedron. ,vol. 66, pp. 5373- 5377 ,(2010) , 10.1016/J.TET.2010.05.054
Chhanda Mukhopadhyay, Arup Datta, Ray J. Butcher, Highly Efficient One-Pot, Three-Component Mannich Reaction Catalyzed by Boric Acid and Glycerol in Water with Major “syn” Diastereoselectivity. ChemInform. ,vol. 40, ,(2009) , 10.1002/CHIN.200943067
Steven J. Brickner, Michael R. Barbachyn, Douglas K. Hutchinson, Peter R. Manninen, Linezolid (ZYVOX), the First Member of a Completely New Class of Antibacterial Agents for Treatment of Serious Gram-Positive Infections Journal of Medicinal Chemistry. ,vol. 51, pp. 1981- 1990 ,(2008) , 10.1021/JM800038G
A. H. Ford-Moore, 512. Divinyl sulphone and allied compounds Journal of The Chemical Society (resumed). pp. 2433- 2440 ,(1949) , 10.1039/JR9490002433
Azim Ziyaei Halimehjani, Katayoun Marjani, Akram Ashouri, Synthesis of dithiocarbamate by Markovnikov addition reaction in aqueous medium Green Chemistry. ,vol. 12, pp. 1306- 1310 ,(2010) , 10.1039/C004711B
Kristen M. Amore, Nicholas E. Leadbeater, Tyson A. Miller, Jason R. Schmink, Fast, easy, solvent-free, microwave-promoted Michael addition of anilines to α,β-unsaturated alkenes: synthesis of N-aryl functionalized β-amino esters and acids Tetrahedron Letters. ,vol. 47, pp. 8583- 8586 ,(2006) , 10.1016/J.TETLET.2006.09.114
Lei Yang, Li-Wen Xu, Wei Zhou, Lyi Li, Chun-Gu Xia, Highly efficient aza-Michael reactions of aromatic amines and N-heterocycles catalyzed by a basic ionic liquid under solvent-free conditions Tetrahedron Letters. ,vol. 47, pp. 7723- 7726 ,(2006) , 10.1016/J.TETLET.2006.08.103
Mihir K. Chaudhuri, Sahid Hussain, M. Lakshmi Kantam, B. Neelima, Boric acid: a novel and safe catalyst for aza-Michael reactions in water Tetrahedron Letters. ,vol. 46, pp. 8329- 8331 ,(2005) , 10.1016/J.TETLET.2005.09.167
Jiong Jack Chen, Cuong V. Lu, Rebecca N. Brockman, Catalyzed double Michael addition of anilines to vinyl sulfone Tetrahedron Letters. ,vol. 44, pp. 3459- 3462 ,(2003) , 10.1016/S0040-4039(03)00702-0