Synthesis of metastable γ-manganese sulfide crystallites by microwave irradiation
作者： ShuBo Wang , KunWei Li , Ran Zhai , Hao Wang , YuDong Hou
DOI: 10.1016/J.MATCHEMPHYS.2004.11.027
关键词:
摘要: Abstract Metastable wurtzite-type (γ) manganese sulfide (MnS) crystallites were obtained by the reaction between acetate and thioacetamide under microwave irradiation in dilute aqueous ammonia within 20 min. The samples characterized X-ray diffraction (XRD) scanning electron microscope (SEM). It shows that time additive tri-ethanolamine (TEA) play important role eliminating MnOx impurities favoring formation of γ-MnS.
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sci-hub.se 参考文章(10)
K. J. Rao, B. Vaidhyanathan, M. Ganguli, P. A. Ramakrishnan, Synthesis of inorganic solids using microwaves Chemistry of Materials. ,vol. 11, pp. 882- 895 ,(1999) , 10.1021/CM9803859
B. J. Skromme, Y. Zhang, David J. Smith, S. Sivananthan, Growth and characterization of pseudomorphic single crystal zinc blende MnS Applied Physics Letters. ,vol. 67, pp. 2690- 2692 ,(1995) , 10.1063/1.114294
Masanobu Nakayama, Kyouhei Watanabe, Hiromasa Ikuta, Yoshiharu Uchimoto, Masataka Wakihara, Grain size control of LiMn2O4 cathode material using microwave synthesis method Solid State Ionics. ,vol. 164, pp. 35- 42 ,(2003) , 10.1016/J.SSI.2003.08.048
L. Wang, S. Sivananthan, R. Sporken, R. Caudano, Interface properties and valence-band discontinuity of MnS/ZnSe heterostructures Physical Review B. ,vol. 54, pp. 2718- 2722 ,(1996) , 10.1103/PHYSREVB.54.2718
S.W. Kennedy, K. Harris, E. Summerville, Mechanisms of thermal transformation of zinc blende to [NaCl] in MnS crystals Journal of Solid State Chemistry. ,vol. 31, pp. 355- 359 ,(1980) , 10.1016/0022-4596(80)90099-7
YongCai Zhang, Hao Wang, Bo Wang, HaiYan Xu, Hui Yan, Masahiro Yoshimura, Hydrothermal synthesis of metastable γ-manganese sulfide crystallites Optical Materials. ,vol. 23, pp. 433- 437 ,(2003) , 10.1016/S0925-3467(02)00334-8
Heribert Wiedemeier, A.Gary Sigai, Vapor transport and crystal growth in the mixed system MnS-MnSe Journal of Crystal Growth. ,vol. 6, pp. 67- 71 ,(1969) , 10.1016/0022-0248(69)90094-3
Tao Ding, Jian-Rong Zhang, Su Long, Jun-Jie Zhu, Synthesis of HgS and PbS nanocrystals in a polyol solvent by microwave heating Microelectronic Engineering. ,vol. 66, pp. 46- 52 ,(2003) , 10.1016/S0167-9317(03)00023-6
Jun-Jie Zhu, Hui Wang, Jian-Ming Zhu, Jun Wang, A rapid synthesis route for the preparation of CdS nanoribbons by microwave irradiation Materials Science and Engineering B-advanced Functional Solid-state Materials. ,vol. 94, pp. 136- 140 ,(2002) , 10.1016/S0921-5107(01)01047-9
Jun Lu, Pengfei Qi, Yiya Peng, Zhaoyu Meng, Zhiping Yang, Weichao Yu, Yitai Qian, Metastable MnS Crystallites through Solvothermal Synthesis Chemistry of Materials. ,vol. 13, pp. 2169- 2172 ,(2001) , 10.1021/CM010049J