Characterization of peanut oil tricacyglycerols by HPLC, GLC and EIMS

作者: J. A. Singleton , H. E. Pattee

DOI: 10.1007/BF02636389

关键词:

摘要: Twenty-three peanut oil triacylglycerols have been characterized by liquid chromatography, gas chromatography and electron impact mass spectrometry. High resolution was achieved using two 8-cm × 6.2-mm reverse phase columns in series, 20 of the were separated an analysis time less than 45 min. Triacylglycerols identified analyzing each fraction for carbon number, fatty acid composition fragmentation pattern. The combined application these methods permitted identification representing combinations all acids present oil.

参考文章(13)
C. Merritt, M. Vajdi, S. G. Kayser, J. W. Halliday, M. L. Bazinet, Validation of computational methods for triglyceride composition of fats and oils by liquid chromatography and mass spectrometry Journal of the American Oil Chemists' Society. ,vol. 59, pp. 422- 432 ,(1982) , 10.1007/BF02634427
J. A. Singleton, H. E. Pattee, Retention behavior of triglycerides on reverse phase columns using pseudophase liquid chromatography Journal of the American Oil Chemists' Society. ,vol. 62, pp. 739- 742 ,(1985) , 10.1007/BF03028743
J. A. Singleton, H. W. Pattee, Optimization of parameters for the analysis of triglyceride by reverse phase HPLC using a UV detector at 210 nm Journal of the American Oil Chemists' Society. ,vol. 61, pp. 761- 766 ,(1984) , 10.1007/BF02672130
G. Sempore, J. Bezard, Triacylglycerol structure of an african peanut oil Journal of the American Oil Chemists Society. ,vol. 59, pp. 124- 129 ,(1982) , 10.1007/BF02662257
Kathleen Payne-Wahl, Gayland F. Spencer, Ronald D. Plattner, Royden O. Butterfield, High-performance liquid chromatographic method for quantitation of free acids, mono-, di- and triglycerides using an infrared detector Journal of Chromatography A. ,vol. 209, pp. 61- 66 ,(1981) , 10.1016/S0021-9673(00)80423-9
M. W. Dong, J. L. Dicesare, Improved separation of natural oil triglycerides by liquid chromatography using columns packed with 3-μm particles Journal of the American Oil Chemists' Society. ,vol. 60, pp. 788- 791 ,(1983) , 10.1007/BF02787428
W. M. Lauer, A. J. Aasen, G. Graff, R. T. Holman, Mass spectrometry of triglycerides: I. Structural effects Lipids. ,vol. 5, pp. 861- 868 ,(1970) , 10.1007/BF02531117