Gel growth and characterization of bismuth oxalate single crystals

作者: G. Polla , R.F. Baggio , E. Manghi , P.K. De Perazzo

DOI: 10.1016/0022-0248(84)90131-3

关键词:

摘要: Abstract The simultaneous growth of Bi 2 ( C O 4 ) 3 ·7 H and · single crystals, by two different techniques (slow evaporation from solution gel growth) is reported. work includes a comprehensive characterization for both compounds, performed on the much better grown specimens, as well crystal powder X-ray data thorough study thermal behaviour. Dominant hillocks giving rise to vicinal faces in are described, tentative explanation their existence given.

参考文章(12)
A.S. Khan, T.C. Devore, Wilfred F. Reed, Growth of the transition metal oxalates in gels Journal of Crystal Growth. ,vol. 35, pp. 337- 339 ,(1976) , 10.1016/0022-0248(76)90199-8
H.J. Scheel, D. Elwell, Surface features on flux-grown refractory oxide crystals Journal of Crystal Growth. ,vol. 20, pp. 259- 267 ,(1973) , 10.1016/0022-0248(73)90089-4
W.J.P. van Enckevort, L.A.M.J. Jetten, Surface morphology of the {010} faces of potassium hydrogen phthalate crystals Journal of Crystal Growth. ,vol. 60, pp. 275- 285 ,(1982) , 10.1016/0022-0248(82)90100-2
H. Arend, J.J. Connelly, Tetramethoxysilane as gel forming agent in crystal growth Journal of Crystal Growth. ,vol. 56, pp. 642- 644 ,(1982) , 10.1016/0022-0248(82)90048-3
F. Lefaucheux, M.C. Robert, E. Manghi, A comparison between gel grown and solution grown crystals — case of ADP and KDP Journal of Crystal Growth. ,vol. 56, pp. 141- 150 ,(1982) , 10.1016/0022-0248(82)90022-7
S. K. Arora, Tomy Abraham, R. S. Godbole, D. Lakshminarayana, Electrical conductivity and dehydration steps of gel-grown CdC2O4·3H2O Journal of Materials Science. ,vol. 18, pp. 57- 63 ,(1983) , 10.1007/BF00543810
S.K. Arora, Tomy Abraham, Controlled nucleation of cadmium oxalate in silica hydrogel and characterization of grown crystals Journal of Crystal Growth. ,vol. 52, pp. 851- 857 ,(1981) , 10.1016/0022-0248(81)90388-2
H. Küppers, Die züchtung grosser einkristalle von kalium- und ammoniumoxalaten Journal of Crystal Growth. ,vol. 15, pp. 89- 92 ,(1972) , 10.1016/0022-0248(72)90128-5
F. Lefaucheux, M.C. Robert, E. Manghi, H. Arend, X-ray characterization of gel grown CaHPO4·2 H2O and PbHPO4 crystals Journal of Crystal Growth. ,vol. 51, pp. 551- 556 ,(1981) , 10.1016/0022-0248(81)90436-X