Kinetic study of meso‐tetraphenylporphyrin synthesis under microwave irradiation
作者： Rodrigo De Paula , Maria A. F. Faustino , Diana C.G.A. Pinto , Maria G.P.M.S. Neves , José A. S. Cavaleiro
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摘要: A typical synthesis of meso-tetraphenylporphyrin was carried out from condensation pyrrole with benzaldehyde in acidic medium under microwave irradiation. batch tests were and a systematic evaluation organic acid, reactant concentration, power, time reaction, presence added oxidant at normal pressure conditions closed vessels system, allowed us to find good set within the range study. The best result achieved only 5 minutes irradiation showing great reduction reaction reaching yields higher than those mentioned literature for classical synthetic heating method.
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