Pyridinolysis of O-Aryl Phenylphosphonochloridothioates in Acetonitrile
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DOI: 10.5012/BKCS.2008.29.9.1769
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摘要: -Aryl Phenylphosphono-chloridothioates, were prepared by the following single-stepreaction. The equimolar starting materials of phenylthio-phosphonic dichloride, substituted phenols, and triethylamine mixed stirred in methylene chloride solventfor 2 hrs, all kept an ice bath.GR grade dichloride (TCI, Japa n), andtriethylamine (Aldrich) used without further purifi-cation. physical constants substrates asfollows:
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