Dispersive solid‐phase extraction of buprenorphine from biological fluids using metal‐organic frameworks and its determination by ultra‐performance liquid chromatography
作者： Farzaneh Mohammadi , Ali Mohammad Haji Shabani , Shayessteh Dadfarnia , Mehdi Ansari , Ali Akbar Asgharinezhad
关键词:
摘要: In this work, various types of metal-organic frameworks were synthesized, and their affinities toward buprenorphine evaluated using dispersive solid-phase extraction. The extracted was determined by ultra high performance liquid chromatography-ultraviolet detection system. highest extraction recovery observed employing zeolitic imidazole framework-67. Then, a facile fast method designed for the purification target drug. Optimization carried out design experiment approach. A linearity range 1-1000 μg/L with limit 0.15 relative standard deviations (50 μg/L, n = 5) 3.4% obtained sample analysis. Under optimized experimental instrumental conditions, recoveries in 95 to 111%. Eventually, framework-67 successfully employed determination biological fluids satisfactory results.
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