Determination of volatile components in peptic powder by gas chromatography-mass spectrometry and chemometric resolution.
作者： Fan Gong , Yi-Zeng Liang , Hui Cui , Foo-Tim Chau , Benny Tsz-Pun Chan
DOI: 10.1016/S0021-9673(00)01098-0
关键词:
摘要: Gas chromatography-mass spectrometry (GC-MS) coupled with chemometric resolution upon two-dimensional data was proposed as a method for the analysis of volatile components in traditional Chinese medicinal preparation peptic powder which contains Rhizoma Atractylodis, Pericarpium Citri Reticulatae, Cortex Magnoliae Officinalis and Radix Glycyrrhizae. Ninety-three were separated 65 them qualitatively quantitatively analyzed represented about 90.28% total content. With help resolution, resolved into pure chromatogram mass spectrum each chemical component. The accuracy qualitative quantitative results greatly improved by using comprehensive information chromatograms spectra. example showed that could enhance separation ability. This makes it possible to analyze complicated practical systems like preparations instruments methods.
elsevier.com
sci-hub.se 参考文章(26)
Olav M. Kvalheim, Frode. Brakstad, Yizeng. Liang, Preprocessing of analytical profiles in the presence of homoscedastic or heteroscedastic noise Analytical Chemistry. ,vol. 66, pp. 43- 51 ,(1994) , 10.1021/AC00073A010
Marcel Maeder, Andreas D. Zuberbuehler, The resolution of overlapping chromatographic peaks by evolving factor analysis Analytica Chimica Acta. ,vol. 181, pp. 287- 291 ,(1986) , 10.1016/S0003-2670(00)85248-4
Marcel Maeder, Arne Zilian, Evolving factor analysis, a new multivariate technique in chromatography Chemometrics and Intelligent Laboratory Systems. ,vol. 3, pp. 205- 213 ,(1988) , 10.1016/0169-7439(88)80051-0
Rolf Manne, Hailin Shen, Yizeng Liang, Subwindow factor analysis Chemometrics and Intelligent Laboratory Systems. ,vol. 45, pp. 171- 176 ,(1999) , 10.1016/S0169-7439(98)00101-4
William A. Court, John G. Hendel, Jama Elmi, Reversed-phase high-performance liquid chromatography determination of ginsenosides of Panax quinquefolium Journal of Chromatography A. ,vol. 755, pp. 11- 17 ,(1996) , 10.1016/S0021-9673(96)00580-8
Zhouming Zhao, Edmund R. Malinowski, Window factor analysis of methylene blue in water Journal of Chemometrics. ,vol. 13, pp. 83- 94 ,(1999) , 10.1002/(SICI)1099-128X(199903/04)13:2<83::AID-CEM529>3.0.CO;2-2
H.R. Keller, D.L. Massart, Peak purity control in liquid chromatography with photodiode-array detection by a fixed size moving window evolving factor analysis Analytica Chimica Acta. ,vol. 246, pp. 379- 390 ,(1991) , 10.1016/S0003-2670(00)80976-9
Xian-guo He, Long-ze Lin, Matthew W Bernart, Li-zhi Lian, Analysis of alkamides in roots and achenes of Echinacea purpurea by liquid chromatography–electrospray mass spectrometry Journal of Chromatography A. ,vol. 815, pp. 205- 211 ,(1998) , 10.1016/S0021-9673(98)00447-6
Yi Zeng. Liang, Olav M. Kvalheim, Hans R. Keller, D. Luc. Massart, Peter. Kiechle, Fritz. Erni, Heuristic evolving latent projections: resolving two-way multicomponent data. 2. Detection and resolution of minor constituents Analytical Chemistry. ,vol. 64, pp. 946- 953 ,(1992) , 10.1021/AC00032A020
Xian-guo He, Long-ze Lin, Li-zhi Lian, Analysis of flavonoids from red clover by liquid chromatography—electrospray mass spectrometry Journal of Chromatography A. ,vol. 755, pp. 127- 132 ,(1996) , 10.1016/S0021-9673(96)00578-X