Retenion characteristics of several bonded-phase liquid chromatography columns for some polycyclic aromatic hydrocarbons

作者: Kenneth Ogan , Elena Katz

DOI: 10.1016/S0021-9673(00)88423-X

关键词:

摘要: Abstract We have compared the retention of twelve polycyclic aromatic hydrocarbons (PAHs) on columns packed with octadecyl bonded phases from eight different manufacturers. The capacity ratios and selectivity factors were calculated for each compound every column, under conditions isocratic elution identical mobile phase strength similar linear flow velocities. observed a wide range significantly material. These data did not correlate carbon content or surface concentration alkyl groups various stationary phases. also report characteristics these PAHs manufacturing lots silica used one commercial columns.

参考文章(25)
Gert E. Berendsen, Leo de Galan, A Geometrical Model for Chemically Bonded TMS and PDS Phases Journal of Liquid Chromatography & Related Technologies. ,vol. 1, pp. 403- 426 ,(1978) , 10.1080/01483917808060008
Stephen R. Bakalyar, Rod McIlwrick, Elizabeth Roggendorf, Solvent selectivity in reversed-phase high-pressure liquid chromatography Journal of Chromatography A. ,vol. 142, pp. 353- 365 ,(1977) , 10.1016/S0021-9673(01)92050-3
Karl Karch, Imrich Sebestian, István Halász, Preparation and properties of reversed phases Journal of Chromatography A. ,vol. 122, pp. 3- 16 ,(1976) , 10.1016/S0021-9673(00)82233-5
H. Hemetsberger, W. Maasfeld, H. Ricken, The effect of chain length of bonded organic phases in reversed phase high performance liquid chromatography Chromatographia. ,vol. 9, pp. 303- 310 ,(1976) , 10.1007/BF02268831
Kenneth. Ogan, Elena. Katz, Walter. Slavin, Determination of polycyclic aromatic hydrocarbons in aqueous samples by reversed-phase performance liquid chromatography Analytical Chemistry. ,vol. 51, pp. 1315- 1320 ,(1979) , 10.1021/AC50044A044