CHROMATOGRAPHIC FINGERPRINT STUDY ON WATER-SOLUBLE EXTRACTS OF RADIX ISATIDIS, FOLIUM ISATIDIS, AND THEIR PREPARATIONS BY HPLC-DAD TECHNIQUE
作者： Yanhong Shi , Zhiyong Xie , Rui Wang , Shanjun Huang , Yiming Li
DOI: 10.1080/10826076.2011.644053
关键词:
摘要: Reliable, reproducible, and valid fingerprint analysis methods using high-performance liquid chromatography-photodiode array detection (HPLC-DAD) for characteristic bioactive water-solution extracts of Radix Isatidis, Folium their preparations were firstly developed validated. Ninety-three batches samples investigated the common fingerprinting profile water-soluble was established with professional analytical software recommended by State Food Drug Administration (SFDA). The reference chromatogram also generated 24 peaks showing large peak areas good separation from adjacent peaks, total more than 85% areas. Nine chemical components—including cytidine, progoitrin, hypoxanthine, epiprogoitrin, uridine, adenosine, xanthine, gluconapin, R,S-goitrin—were identified as peaks. Hierarchical clustering (HCA) Principal Component Analysis (PCA) perf...
sci-hub.se 参考文章(16)
Fang Jianguo, Wang Wenqing, Hu Ya, Feng Dan, Tang Jie, Influence of Radix isatidis on the endotoxin-induced release of TNF-α and IL-8 from HL-60 cells Journal of Huazhong University of Science and Technology-medical Sciences. ,vol. 25, pp. 546- 548 ,(2005) , 10.1007/BF02896013
Weijun Kong, Yanling Zhao, Limei Shan, Xiaohe Xiao, Weiying Guo, Thermochemical studies on the quantity-antibacterial effect relationship of four organic acids from Radix Isatidis on Escherichia coli growth. Biological & Pharmaceutical Bulletin. ,vol. 31, pp. 1301- 1305 ,(2008) , 10.1248/BPB.31.1301
Wei Zhou, Mei-Fen Xie, Xiao-Yan Zhang, Ting-Ting Liu, Ying-Jia Yu, Geng-Li Duan, Improved liquid chromatography fingerprint of fat‐soluble Radix isatidis extract using multi‐wavelength combination technique Journal of Separation Science. ,vol. 34, pp. 1123- 1132 ,(2011) , 10.1002/JSSC.201000834
P. Zou, Y. Hong, H.L. Koh, Chemical fingerprinting of Isatis indigotica root by RP-HPLC and hierarchical clustering analysis Journal of Pharmaceutical and Biomedical Analysis. ,vol. 38, pp. 514- 520 ,(2005) , 10.1016/J.JPBA.2005.01.022
Wenzhi Zeng, Yanjing Bai, Qingying Zhang, Yuying Zhao, Chromatographic fingerprint analysis of Semen Ziziphi spinosae by HPLC-DAD method. Analytical Letters. ,vol. 42, pp. 205- 215 ,(2009) , 10.1080/00032710802585642
Zhao Liu, Zhan-qiu Yang, Hong Xiao, Antiviral activity of the effective monomers from folium isatidis against influenza virus in vivo Virologica Sinica. ,vol. 25, pp. 445- 451 ,(2010) , 10.1007/S12250-010-3142-0
Eun Kyung Shin, Dae Hwan Kim, Hwan Lim, Hyun-Kyung Shin, Jin-Kyung Kim, The anti-inflammatory effects of a methanolic extract from Radix Isatidis in murine macrophages and mice. Inflammation. ,vol. 33, pp. 110- 118 ,(2010) , 10.1007/S10753-009-9164-9
Jian-guo Fang, Yun-hai Liu, Wen-qing Wang, Wei Xie, Shu-xian Fang, Hong-gang Han, The anti-endotoxic effect of o-aminobenzoic acid from Radix Isatidis. Acta Pharmacologica Sinica. ,vol. 26, pp. 593- 597 ,(2005) , 10.1111/J.1745-7254.2005.00080.X
Xin Zhou, Yang Zhao, Peihai Lei, Zongwei Cai, Hai Liu, Chromatographic fingerprint study on Evodia rutaecarpa (Juss.) Benth by HPLC/DAD/ESI‐MSn technique Journal of Separation Science. ,vol. 33, pp. 2258- 2265 ,(2010) , 10.1002/JSSC.201000035
Zeng Ling, Tcm Factory, Study on fingerprint for the quality control of Banlangen Granule Chinese Traditional Patent Medicine. ,(2004)