A method for sulfonamide medicine extraction and analysis by utilizing a DPX pipette tip type dispersive solid-phase extraction microcolumn
作者： Yang Jia , Fei Jing , Ka Molai , Wang Jue , Wang Qian
DOI:
关键词:
摘要: The invention provides a method for sulfonamide medicine extraction and analysis by utilizing DPX pipette tip type dispersive solid-phase microcolumn, relates to medicineresidue detection methods animal-sourced foods. is provided overcome problem that there no effective foods, especially quantitative, high-precision, high-throughput low-consumption determination. A high performance liquid chromatography-tandem mass spectrometry manner residue of twelve sulfonamidemedicines in foods established the method. suitable amount one or plurality medicines selected from sulfacetamide, sulfapyridine, sulfamerazine, sulfamethazine, sulfamethoxypyridazine, sulfamonomethoxine, sulfochloropyridazine, sulfamethoxazole, sulfadimethoxypyridazine, sulfadimethisoxazol, sulfabenzamide sulfaquinoxalin
lens.org 参考文章(10)
Wei Jia, Lin Shi, Xiaogang Chu, Untargeted screening of sulfonamides and their metabolites in salmon using liquid chromatography coupled to quadrupole Orbitrap mass spectrometry. Food Chemistry. ,vol. 239, pp. 427- 433 ,(2018) , 10.1016/J.FOODCHEM.2017.06.143
Geng Dandan, Tan Liang, Dong Qi, Xiao Yuancan, Chi Xiaofeng, Xu Xu, Hu Fengzu, Method for detecting residual quantity of 18 sulfanilamide drugs in beef and mutton ,(2016)
Peng Fang, Zhu Zitong, Wu Xiaoqin, Lei Meikang, Chen Yujiao, Method for simultaneously measuring 16 sulfonamides in beewax by high performance liquid chromatography tandem mass spectrometry ,(2015)
Li Mei, Zhang Pengfei, Wang Wei, Wang Danhui, Pretreatment method of milk sample for sulfonamides residue detection with liquid chromatography and detection method ,(2016)
Guo Liming, Wang Hongwei, Li Zongjin, Zhang Bao, Rao Qinxiong, Method for detecting drug residues in meat and kit thereof ,(2014)
William Brewer, Wang Qian, Wang Jue, Kamolrat Metavarayuth, Kaylee Mastrianni, Method for extracting and analyzing beta-agonists clenbuterol by adopting DPX (dispersive pipette extraction) tip type dispersive solid-phase microextraction column ,(2017)
Liu Yaxiong, Zhuang Yue, Luo Zhuoya, Rapid screening method for illegally added 132 chemical drugs in Chinese patent medicines and health care products ,(2018)
Zhang Fengyan, Jiang Wanfeng, Method for rapidly screening and certifying veterinary drug residue in milk ,(2018)
Zhao Jinli, Zhong Yuxin, Qiu Peili, Huang Song, Meng Weiwei, Wang Chenglong, Method for detecting 35 veterinary drug residues in meat product at same time ,(2018)
Yuan Zhejun, Zhang Yu, Zhu Ying, Shen Genxiang, Wang Zhenqi, Hu Shuangqing, Qian Xiaoyong, Zhang Hongchang, Method for simultaneously detecting six types of 24 antibiotics in livestock excrements by combination of ultrasonic extraction-solid phase extraction pretreatment and liquid chromatography-mass spectrometry technology ,(2018)