Fast Analysis of Complete Macroscopic Gunshot Residues on Substrates Using Raman Imaging.

作者: Maria López-López , María Ángeles Fernández de la Ossa , Carmen García-Ruiz

DOI: 10.1366/14-07816

关键词:

摘要: Raman spectroscopy has emerged as a viable technique for the organic analysis of gunshot residues (GSRs), offering additional information to well-established using scanning electron microscopy coupled with energy-dispersive X-ray (SEM-EDX). In this article, imaging system an electron-multiplying coupled-charged device (EMCCD) camera was used analyze complete GSR particles from both conventional and nontoxic ammunition fired at different cloth targets. The same cloths were then stained blood mimic real evidence measured. direct collected stubs SEM-EDX (the frequent method collection) evaluated. Multivariate curve-resolution chemical-mapping methods applied spectroscopic data identify highlight signal corresponding differentiate them substrates. It confirmed that measurement approaches (on...

参考文章(18)
María López-López, Juan Jose Delgado, Carmen García-Ruiz, Analysis of macroscopic gunshot residues by Raman spectroscopy to assess the weapon memory effect. Forensic Science International. ,vol. 231, pp. 1- 5 ,(2013) , 10.1016/J.FORSCIINT.2013.03.049
C. Paris, C. Coupry, Fourier transform Raman spectroscopic study of the first cellulose‐based artificial materials in heritage Journal of Raman Spectroscopy. ,vol. 36, pp. 77- 82 ,(2005) , 10.1002/JRS.1288
S. Steffen, M. Otto, L. Niewoehner, M. Barth, Z. Bro¿żek-Mucha, J. Biegstraaten, R. Horváth, Chemometric classification of gunshot residues based on energy dispersive X-ray microanalysis and inductively coupled plasma analysis with mass-spectrometric detection Spectrochimica Acta Part B: Atomic Spectroscopy. ,vol. 62, pp. 1028- 1036 ,(2007) , 10.1016/J.SAB.2007.04.005
Anna de Juan, Romà Tauler, Multivariate Curve Resolution (MCR) from 2000: Progress in Concepts and Applications Critical Reviews in Analytical Chemistry. ,vol. 36, pp. 163- 176 ,(2006) , 10.1080/10408340600970005
Justin Bueno, Igor K. Lednev, Attenuated total reflectance-FT-IR imaging for rapid and automated detection of gunshot residue. Analytical Chemistry. ,vol. 86, pp. 3389- 3396 ,(2014) , 10.1021/AC4036718
Désiré Laza, Bart Nys, Jan De Kinder, Andrée Kirsch-De Mesmaeker, Cécile Moucheron, Development of a quantitative LC-MS/MS method for the analysis of common propellant powder stabilizers in gunshot residue. Journal of Forensic Sciences. ,vol. 52, pp. 842- 850 ,(2007) , 10.1111/J.1556-4029.2007.00490.X
José Manuel Amigo, Practical issues of hyperspectral imaging analysis of solid dosage forms Analytical and Bioanalytical Chemistry. ,vol. 398, pp. 93- 109 ,(2010) , 10.1007/S00216-010-3828-Z
Zuriñe Abrego, Nagore Grijalba, Nora Unceta, Maite Maguregui, Alicia Sanchez, Alberto Fernández-Isla, M. Aranzazu Goicolea, Ramón J. Barrio, A novel method for the identification of inorganic and organic gunshot residue particles of lead-free ammunitions from the hands of shooters using scanning laser ablation-ICPMS and Raman micro-spectroscopy Analyst. ,vol. 139, pp. 6232- 6241 ,(2014) , 10.1039/C4AN01051E
Justin Bueno, Vitali Sikirzhytski, Igor K. Lednev, Raman spectroscopic analysis of gunshot residue offering great potential for caliber differentiation. Analytical Chemistry. ,vol. 84, pp. 4334- 4339 ,(2012) , 10.1021/AC203429X